HM50 4th Ed - Tank Cleaning Guide - For Cross Reference

Hydrocarbon management

HM 50

Guidelines for the cleaning of tanks

and lines for marine tank vessels carrying
petroleum and refined products
4th edition
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HM 50 GUIDELINES FOR THE CLEANING OF TANKS AND LINES
FOR MARINE TANK VESSELS CARRYING PETROLEUM
AND REFINED PRODUCTS
Fourth edition
May 2017
Published by
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HM 50 GUIDELINES FOR THE CLEANING OF TANKS AND LINES FOR MARINE TANK VESSELS
CARRYING PETROLEUM AND REFINED PRODUCTS
CONTENTS
Page
Foreword . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3
Acknowledgements . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
1 Introduction and scope . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5
2 Tank cleaning guidelines . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6

2.1 General information . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6
2.1.1 Introduction and cleanliness standards . . . . . . . . . . . . . . . . . . . . . . . . . . . 6
2.1.2 Inert gas . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6
2.1.3 Static electricity . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6
2.2 Bottom and line flushing . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
2.2.1 General . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
2.2.2 Fuel oil cargoes . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
2.3 Elimination of water for critical cargoes . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
2.4 Disposal of residues . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8
2.4.1 Cargo residues . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8
2.4.2 Scale and solid residues . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8
2.5 Tank washing . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9
2.5.1 General . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9
2.5.2 After black oil cargoes . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9
2.5.3 After white oil/clean product cargoes . . . . . . . . . . . . . . . . . . . . . . . . . . . 10
2.5.4 After crude oil cargoes . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10
2.5.5 After vegetable oil cargoes . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10
2.5.6 After fatty acid methyl ester (FAME) or blended biodiesel cargoes . . . . . . 11
2.5.7 After gasoline/ethanol blended cargoes . . . . . . . . . . . . . . . . . . . . . . . . . . 11
2.5.8 Use of chemicals . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11
2.5.9 Cleaning of sampling equipment and stilling wells . . . . . . . . . . . . . . . . . 12
2.6 Tank inspections . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12
2.6.1 General . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12
2.6.2 Inerted tanks . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12
2.7 Heating coils . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12
2.7.1 Testing . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12
2.7.2 Heating coils made from copper-containing alloys . . . . . . . . . . . . . . . . . . 13
2.8 Tank coatings . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13
2.8.1 Temperature restrictions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13
2.8.2 Coating compatibility . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13
2.8.3 Stainless steel . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14
2.8.4 Coating condition . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14
2.9 Cargo lines . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14
2.9.1 General . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14
2.9.2 Cargo compatibility . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14
2.9.3 Testing of cargo lines and valves . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15
2.10 Tank cleaning . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15
2.11 Comments on individual cargoes (cargo types) . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16
Contents continued
Page
2.11.1 Naphthas and light distillate feedstocks (and/or – clean condensate

feedstocks, straight run benzene, pentane, natural gasoline,
straight run gasoline) �� 16
2.11.2 Aviation gasoline (and/or – avgas, aviation spirit) and aviation
turbine gasoline, wide cut jet fuel, JP4, Jet B) �� 16
2.11.3 Leaded motor gasoline (and/or - premium/regular motor spirit,
motor gasoline, mogas) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17
2.11.4 Unleaded motor gasoline (and/or – unleaded motor spirit, regular
unleaded, premium unleaded, super unleaded, toluene,
methyl tertiary butyl ether (MTBE), reformate, alkylate, cracked spirit,
ethanol,motor spirit/gasoline blending components) �� 17
2.11.5 Ultra low sulfur gasolines . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17
2.11.6 Solvents (and/or – special boiling point solvents, rubber solvent,
unleaded cleaning spirit, white spirit) . . . . . . . . . . . . . . . . . . . . . . . . . . . 18
2.11.7 Aviation jet fuel (and/or – aviation kerosene, dual purpose kerosene,
Jet, Jet-A1, Avtur, ATK, JP5, JP8, synthetic jet fuel) . . . . . . . . . . . . . . . . . . 18
2.11.8 Premium and regular kerosenes (and/or – kerosene feedstock,
burning oil, stove oil automotive diesel oil, DERV, extra light fuel oil,
distillate marine diesel . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19
2.11.9 Gas oil and automotive diesel fuel (and/or - automotive gas oil,
automotive diesel oil, DERV, extra light fuel oil, distillate marine diesel) . . 19
2.11.10 Ultra low sulfur automotive diesel fuel (and/or – ULSD,
ULS turbine gas oil, LS marine gas oil, ULS diesel) �� 20
2.11.11 Crude oil and condensate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20
2.11.12 Base lubricating oils . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 21
2.11.13 Vacuum gas oil (and/or – cracker feed, waxy distillate) . . . . . . . . . . . . . . . 21
2.11.14 Medium and heavy fuel oils . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 21
2.11.15 Low sulfur fuel oil (and/or – low sulfur atmospheric residue (LSAR),
low sulfur waxy residue (LSWR)) �� 21
2.11.16 Light fuel oil . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 21
2.11.17 Gas to liquids (GTL) products . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 22
2.11.18 FAME and blended biodiesel . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 22
2.11.19 Light cycle oil (LCO) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 22
Table 1 Cleaning recommendations . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 23
Annexes
Annex A Glossary of terms . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 25
Annex B References . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 28
FOREWORD
The Energy Institute (EI) Hydrocarbon Management Committee is responsible for the production and
maintenance of standards and guidelines covering various aspects of static and dynamic measurement
of petroleum. The Hydrocarbon Management Subcommittee 4 (HMC-4) deals primarily with the
measurement and loss of crude oil and oil products, focusing in particular on transport in the marine
environment.
HMC-4 is made up of experts from the oil industry, cargo inspectors, ship owners and representatives
from marine terminals. It is a truly international panel with representatives from most Western European
countries, the Middle East, Far East and North and South America. Equipment manufacturers and
experts with specific knowledge of measurement techniques are regularly invited to present papers
to the committee.
The EI maintains liaison with parallel working groups of the American Petroleum Institute's Committee
on Petroleum Measurement, and other organisations concerned with quantitative measurement in
other countries and in other industries. The API are permanent invitees to meetings of the HMC-4
committee.
The EI Hydrocarbon Management guidelines (formerly Petroleum Measurement Manual and Petroleum
Measurement papers) are widely used by the petroleum industry and have received recognition in
many countries by consumers and the authorities. In order to promote international good practice the
EI works via the British Standards Institute to develop standards through the International Standards
Organization’s technical committee TC-28 Petroleum Products and related products of synthetic or
biological origin and its subcommittee TC28/SC2 Measurement of petroleum and related products.
A full list of Hydrocarbon Management guidelines is available on request from the EI. The EI
Hydrocarbon Management guidelines are recommended for general adoption but should be read
and interpreted in conjunction with safety, environmental, weights and measures, customs and
excise and other regulations in force in the particular country in which they are to be applied. Such
regulatory requirements have precedence over corresponding clauses in the EI document except
where the requirements of the latter are more rigorous, when its use is recommended. Users should
also consider contractual constraints imposed by charterers, cargo owners, ship owners and any
other interested party.
Although it is believed that adoption of the recommendations of this guideline will assist the user,
the EI cannot accept any responsibility, of whatsoever kind, for damage or alleged damage arising
or otherwise occurring on vessels or in or about premises where this document has been applied,
as final responsibility for adequate preparation of the vessel to receive a cargo lies with the parties
controlling this task.
Users of these guidelines are invited to send comments, suggestions, or details of relevant experience
to:
Technical Department, Hydrocarbon Management

Energy Institute
61 New Cavendish Street
London
W1G 7AR
United Kingdom
e:[email protected]
ACKNOWLEDGEMENTS
Members of the EI Hydrocarbon Management Committee 4 have been associated with the production
of these guidelines. Membership at the time of publication is as follows:
Bazan Group (Oil Refinieries Limited)

BG Group
BP Oil International Ltd
ConocoPhillips Company
CEPSA
Chevron Products Company
China International United Petroleum & Chemicals Co. Ltd (Unipec)
Chinese Petroleum Corporation
CITGO Petroleum Corporation
ENI Trading and Shipping
ERG Petroli
ExxonMobil Refining and Supply Company
Koch Supply and Trading
Marathon Petroleum Company
Mercuria
Petrobras
Petrogal
Petroineos
Phillips 66 Limited
PMI Pemex
Repsol
Saras SpA
Saudi Aramco
Shell
Statoil
Sumed
Total
Valero Marketing and Supply Company
The International Federation of Inspection Agencies provided support via the working group.
Aviation Fuel Management issues have been reviewed by the Joint Inspection Group (JIG) Product
Quality Committee whose contribution is also appreciated.
The guidelines were compiled by Melverley Consultants Limited.
1 INTRODUCTION AND SCOPE
This publication has been compiled with the aim of sharing the experiences of oil companies
and other bodies represented on the HMC-4 with other branches of the oil industry, by
providing guidance with regard to cleaning and washing of tanks on board petroleum tank
vessels, particularly when carrying refined products and changing from one product to
another.
Although the guidelines are written principally for sea-going ships they may also be applied
to inland barges.
This document addresses issues relating to most classes of refined product but does not cover
chemicals or gases.
Guidelines for crude oil washing are contained in HM 40 Guidelines for the crude oil washing
of ships' tanks and the heating of crude oil being transported by sea, published by the EI.
Instructions regarding washing are normally issued by the charterers or vessel owners either
in the form of a specific instruction or a general tank cleaning guideline provided on board.
This publication is intended to provide additional guidance to those involved with issuing such
instructions and to other parties who may be involved in confirming that suitable procedures
have been followed.
This publication has been prepared primarily with the aim of maintaining product quality
through the use of minimum effective tank washing procedures.
Further information relating to handling and quality of aviation fuels can be found in EI/
JIG 1530 Quality assurance requirements for the manufacture, storage and distribution of
aviation fuels to airports.
Safety and environmental issues are paramount in the operations described and for detailed
guidance on these issues the latest revisions of ISGOTT, ISGINTT, MARPOL and SOLAS
regulations should be referred to and will take precedence over any recommendations made
here.
Nothing in the guidance contained in these guidelines suggests or encourages deviation

from the carriage and cleaning requirements required by MARPOL Annex II Noxious Liquid
Substance (NLS) regulations. MARPOL Annex II elevates the carriage and cleaning standards
for specific cargoes. The cleaning standards, carriage requirements and slop disposal provisions
of MARPOL are developed to protect the environment, not necessarily to prepare a tank for
the next cargo. Products addressed in these guidelines to which Annex II NLS regulations
may apply include but are not limited to: biodiesels, lube additives, toluene, methanol, MTBE,
all vegetable oils, and many gasoline blending components.
This fourth edition has dispensed with previous Tables 1, 2, and 3, moving their content
into the main text. The cleaning table, now Table 1, has been significantly revised. The
recommendations acknowledge that enhanced stripping and drying may be an acceptable
alternative to mopping. Some comments on inert gas systems were considered out of scope
and have been removed.
2 TANK CLEANING GUIDELINES
2.1 GENERAL INFORMATION
2.1.1 Introduction and cleanliness standards
Tank cleaning is carried out to:

−− Prepare tanks for the carriage of the next cargo.
−− Prevent the build-up of oily residues.
−− Facilitate gas-freeing and tank entry for repairs/tank mopping.
−− Comply with charter party requirements.
−− Comply with MARPOL regulations.
−− In extreme circumstances, prepare tanks for the carriage of clean ballast.
It can be accomplished by means of portable or fixed tank washing machines, or sometimes

a combination of both using hot, cold, fresh or sea water and/or tank cleaning chemicals
singly or in combination.
In order to reduce unnecessary bunker consumption, impact on the environment and

associated costs, vessels should only tank clean when necessary. Also, introducing water into
the cargo system is not always the best action as it can increase contamination if tanks and
lines are not properly cleared.
Cargo tanks should be cleaned to the standard necessary to meet the requirements for the
next cargo or, where applicable, for clean ballast or for tank-entry and repairs. The tank
cleaning Table 1 is to be used as a guide to the degree of cleaning necessary between
cargoes.
Depending on the intended use of the product concerned, the standard of cleanliness required
by some charterers/receivers may be different from that found within these guidelines. It
is therefore extremely important to ensure that cleaning recommendations are provided in
writing. Any deviations from recommendations should be confirmed in writing.
2.1.2 Inert gas
The inert gas system, where fitted, should be operated appropriately during tank washing,
gas-freeing and tank preparation operations. Additional safety precautions should be taken
for vessels which do not have inert gas systems, although the tank washing recommendations
provided in this document still apply. Safety recommendations contained in ISGOTT should
be followed.
Inert gas systems and scrubbers which are not operated correctly or are poorly maintained
can result in cargo contamination with water, soot, SO2 or SO3. For aviation jet fuel cargo this
can lead to filtration issues and reduce the effectiveness of static dissipators.
2.1.3 Static electricity
Precautions to prevent static discharge during washing operations should be followed at all
times. These are detailed in ISGOTT.
Particularly hazardous conditions may exist when washing under non-inert conditions or
when using hot water wash which can increase the temperature of cargo residues closer to
their flashpoint.
2.2 BOTTOM AND LINE FLUSHING
2.2.1 General
It may be acceptable to flush the tank bottoms with the next grade to be loaded. This flushing
medium is normally then discharged ashore or segregated on board. Discharges to shore can
only take place after discussion with all parties involved. There will be costs associated with
this procedure (in particular the flushing medium), and all parties will need to agree to these
costs and how they are to be met.
Flushing pumps and lines using water can only be considered when suitable reception
facilities are available ashore or where washings can be pumped to a suitable slops tank. On
completion, all lines and pumps should be well drained, but the practice of draining to the
pump room bilge should be avoided.
2.2.2 Fuel oil cargoes
When changing from a higher quality product to a lower quality product (e.g. low to high
sulfur), it may be possible, under certain circumstances, to reduce the tank preparation
procedures. In these cases, the ROB should still be minimised.
Provided that any contamination would not adversely alter the quality of the cargo to be
loaded, then load on top may be possible. However, this matter should always be clarified
with, and agreed to by, all interested parties. Where uncertainty exists, the tank washing
guidelines should be followed.
When loading vacuum gas oil/waxy distillate or other feedstock products, it will be necessary
to remove salt residues from any tank which has previously contained salt water ballast or has
been cleaned using salt water (see Table 1), typically using a fresh water rinse.
2.3 ELIMINATION OF WATER FOR CRITICAL CARGOES
When it is necessary to mop tanks dry for critical cargoes such as aviation kerosene, lubricating
oil, or FAME, care should be taken to achieve a compatible standard of preparation throughout
that portion of the cargo system allocated to the critical product. The following procedures
should be followed:
The cargo lines which are to load and discharge the critical product should be opened and
well drained. This includes manifolds, drop lines, pump discharge lines and tank suction lines.
Cargo pumps and their associated air vessels, strainers and bypasses should be opened and
well drained. This is to include any vacuum breakers.
Individual tank suction valves should be opened and remain open during the mopping
process. Valve inspection covers should be opened as necessary.
Where fitted, fixed eductor systems should be blown through with air, valves opened and
lines left to drain into the tank prior to mopping.
Fixed tank washing lines should be drained, and any water in the leg between the main line
and the machine allowed to drain into the tank via the machine prior to mopping.
After draining, the fixed tank cleaning machines should be positively isolated from the supply
line by blanking or other secure means.
Particular attention should be paid to the inert gas deck seal overboard line. It should be
ascertained that this line is free from blockage and that there are no valves partially or
fully closed. Any substantial increase in the deck seal water level will cause 'carry over' and
introduce water back into the tank during re-inerting.
Low point drains on inert gas lines should be cleared of water and other liquid contamination.
Condensed liquids in the inert gas lines can be hazardous.
As a general rule when loading, the product should be directed initially into a single tank
using as many lines as possible. This will ensure that any water trapped in the system will
be flushed through to this single tank. The water is then much easier to deal with at the
discharge port if necessary. However, this procedure should be verified with the charterers.
2.4 DISPOSAL OF RESIDUES
2.4.1 Cargo residues
Ballast residues remaining on crude oil and black oil carriers should be retained on board.
Vessels loading crude oil may load on top of these residues provided they receive permission
from the cargo owner or charterer. Black oil carriers should discharge the residues to shore
reception facilities, when they are available; otherwise, they should retain them on board,
segregated from the cargo until such times as it is possible to either load on top or discharge
to a shore facility.
Residues should be dealt with in compliance with current MARPOL regulations to reduce the
quantity of residues on board. When shore reception facilities are available at the loading
port, residues should be discharged to the facilities. If they are not available, residues should
be retained on board, segregated from the cargo.
2.4.2 Scale and solid residues
Scale and solid residues on the horizontal surfaces within a tank can contain volatile liquids
and generate gas when disturbed. On crude oil carriers the build-up of sludge deposits can be
controlled by effective crude oil washing. On other ships, routine water washing can be used.
When sludge has to be physically removed from tanks, it shall not be disposed of overboard
at sea but should be bagged, accurately labelled and landed to shore reception facilities. In
coated tanks scale should be minimal, unless significant coating breakdown occurs.
2.5 TANK WASHING
2.5.1 General
Appropriate stern trim and efficient use of washing equipment are important. Minimum tank
washing patterns should be used. Any accumulations of scale should be removed frequently,
and excessive coating break-down leading to build-up of scale should be recorded.
2.5.2 After black oil cargoes
These cargoes range from gas oils to heavy fuel oils and the degree of cleaning will vary
considerably with the grade to be loaded and the grades previously carried. Products within
this group are persistent oils and residues and should be handled in accordance with 2.4.
If the ship is reloading at the discharge port, it may be possible to pump washings/residues
from tank cleaning operations to a shore facility. Otherwise, the residues will be retained on
board. Regardless of the medium used for washing (cargo or water), care should be taken to
ensure that segregation is not compromised.
Heavy fuel oils may leave residues on tank bottoms and structures at low temperatures and
these can cause serious contamination of the lighter fuels and gas oils. Washing should be
continued until the required degree of cleanliness is achieved. The bottom portion of the
tank, together with any internal structure, may require particular attention, especially after
carrying heavy or waxy fuel oils. Where available, portable tank cleaning machines may be
required to ensure adequate coverage.
Hot water should always be used when the nature of the cargo warrants it or when a special
degree of cleaning is required. The temperature of any residues should be at least 15 °C
above the pour point in order to achieve effective removal by tank washing.
Scale formation is not usually heavy in ships which are employed solely on black oil trading,
but where present it may be mixed with waxy deposits from fuel oils, which make it difficult
to clean to the standard for gas oils and light fuel oils, etc. If a build-up occurs special
arrangements may need to be made to remove or reduce these deposits.
The amount of washing required when changing from a black oil cargo to a white oil cargo
cannot be defined precisely as it varies considerably and depends primarily on the length
of time the vessel was in the black oil trade, the condition of the tank coating and the
arrangement of the cleaning machines within the tanks. In the best of situations it might take
as little as four hours per tank; however, under less than ideal circumstances it can take many
times longer. It is particularly important to ensure that blind areas under structures are
adequately washed.
After the initial washing, the tank should be gas-freed and inspected to check on the
effectiveness of the washing.
One of the major causes of tanks not being washed properly is poor monitoring of machines.
They are prone to sticking, so that the nozzles fail to rotate in the vertical plane and the
body fails to rotate in the horizontal plane. This results in the majority of the structure being
washed only by splashing. Poor washing may also be caused by poor stripping – failure
to remove water from the tank during the wash. This can be due to a number of factors
including insufficient trim, adverse list, or the pumps not keeping up with the water being
added to the tank.
2.5.3 After white oil/clean product cargoes
White oil cargoes range from very light volatile oils like naphtha, to gas oils and lubricating
oils.
Cold water washing is generally adequate for cleaning after most white oil cargoes, except
after the carriage of the heavier lubricating oils where hot water or chemical wash may be
required. Also, the risk of contamination of certain grades may require the removal of all
previous cargo (see Table 1).
Although it is often important to remove all traces of the last cargo, it is also important
to avoid excess tank washing, particularly with hot water, as this may eventually lead to
expensive renewal of tank coatings. Providing that the coatings are in a good condition,
adhesion of most types of clean oil is minimal and this reduces the amount of washing
required.
With volatile cargoes, little residue is left on tank sides and structure other than liquid and
gases trapped in scale and other loose materials. With gas oils and lubricating oils an oily film
will remain. With all cargoes, there is also a small amount of liquid left below the effective
stripping level.
2.5.4 After crude oil cargoes
The statutory requirements for washing after crude oils are contained within MARPOL.
Additional sources of information are the vessel's cargo operations manual and EI HM 40.
The following points should be assessed when considering the need for water washing of
crude oil tanks:
−− the build-up of sludge in the tanks;
−− wax content of the crude;
−− the possibility of delaying the washing until the vessel is in warmer water;
−− the use of portable machines, and
−− the next crude to be carried and its suitability for washing.
2.5.5 After vegetable oil cargoes
Vegetable oils can be defined as drying, non-drying and semi-drying.
Non-drying oils are liquid at ambient temperatures and are easy to clean from surfaces using
detergents and degreasers. Iodine values tend to be below 110 (examples are coconut oil,
palm oil, palm kernel oil, olive oil).
Semi-drying oils have iodine values between 110 and 140.
Drying oils create solid residues which can form a hard skin at ambient temperatures. They
are more difficult to remove from surfaces. Iodine values tend to be between 140 and 190
(examples are linseed oil, tung oil).
The drying properties (iodine value) are not related to the melting point so a light oil may well
exhibit drying properties.
10
There are many types of vegetable oil, some of which have chemical additives. Generally,
efforts should be made to remove all traces of such cargoes before loading petroleum
products, as vegetable oil traces may affect not only the next cargo but those following later.
Lighter vegetable oils will typically be cold water washed then washed with warm water and
a degreaser or saponifier. Heavier types may require hot water washing, again with degreaser
or saponifier, followed with a solvent wash. If the previous cargo was a drying oil, then a
hot wash with saponifier followed by additional water washes until the ph is neutral will be
required. Cold water washing of each tank immediately after completion of discharge may
avoid formation of a film on internal tank surfaces and should be carried out before warm or
hot water washes which may cause oil films to dry ('varnish') unless cold water is used first.
See also 2.5.6, 2.11.2 and 2.11.7 regarding loading aviation jet fuel and aviation gasoline
cargoes after biologically-derived products.
2.5.6 After fatty acid methyl ester (FAME) or blended biodiesel cargoes
Analysis has shown that FAMEs adhere to surfaces more readily than other oils. However, as
they remain liquid at ambient temperatures, they can be cleaned using a water wash and
saponifier (type to be recorded in the vessel cleaning log) as described in 2.5.5 for lighter
vegetable oils.
Contamination of aviation kerosene with FAME is a serious concern. Intermediate cargoes

and a strict washing regime are therefore recommended when following these cargoes with
aviation kerosene (see 2.11.7) and special cleaning instructions should be obtained from the
cargo owner.
Note: The recommendations relating to FAME also apply to other fatty acid esters.
2.5.7 After gasoline/ethanol blended cargoes
For tank cleaning purposes these cargoes may be treated in the same way as the equivalent
non-biologically-derived cargoes for non-aviation fuel purposes. Where aviation products are
involved, see 2.11.2 and 2.11.7
2.5.8 Use of chemicals
Due to environmental considerations, tank cleaning chemicals should no longer be used

except where there is a requirement for stringent cleaning, in which case specific instructions
should be issued for chemically-assisted cleaning at the time of the cargo nomination. Where
chemicals are used, details should be recorded in the vessel cleaning log and slops should be
segregated to allow for easier disposal.
Note: The use of saponifiers can cause haze in any hydrocarbon. Tank cleaning chemicals
containing surfactants should not be used to prepare tanks for aviation jet fuel or aviation
gasoline cargoes as residues can cause fixed haze in the fuel and harm aviation fuel filters
(see 2.11.7).
11
2.5.9 Cleaning of sampling equipment and stilling wells
The tight specifications for sensitive grades require extreme care during sampling, particularly
closed or restricted sampling, to avoid contamination from previous cargoes or build-up of
residues. Examples of this are FAME contamination of aviation fuels, and vegetable oils in
gasolines. To reduce the possibility of drawing unrepresentative samples, the cleaning of
sampling equipment, vapour locks, standpipes and stilling wells is recommended as part of
the tank cleaning regime.
2.6 TANK INSPECTIONS
2.6.1 General
Responsibility for the cleanliness and overall suitability of tanks, lines and pumps to carry the
nominated grades lies with the Master. Inspections are frequently carried out by the loading
supervisors from the shore facility or by independent inspectors acting on behalf of the cargo
owner. However, while such inspections may provide an opinion regarding those tanks which
have been inspected, they do not relieve the Master of his/her responsibilities.
Tank entry for inspections is potentially dangerous and should only be done under close
scrutiny in accordance with a strict permit to enter/work system in gas-free tanks. Careful
attention should be given to the need for lighting, access, safety equipment, personal
protective equipment and the general tank environment, e.g. residues on plates (slip hazard),
etc.
2.6.2 Inerted tanks
Any requirement for cargo tank(s) to be gas-freed to allow internal inspection should be
contained within the agreed charter party or voyage orders for the voyage about to be
undertaken as de-inerting/re-inerting is costly and time-consuming.
Reference should be made to ISGOTT recommendations with regard to inerting.
2.7 HEATING COILS
2.7.1 Testing
Heating coils should be pressure tested, and if necessary, blown through and repaired, on
each occasion prior to:
−− Loading a cargo which requires heating.
−− Carrying out tank repairs or tank entry (so that any coil leak will not introduce
hydrocarbon gases or product into the tank).
−− Gas-freeing for voyage repairs or dry-docking.
Similar action should be taken when changing from a low flashpoint to a high flashpoint
cargo or from black oil products to white oil products.
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2.7.2 Heating coils made from copper-containing alloys
Heating coils made from copper-containing alloys can reduce the thermal stability of aviation
kerosene due to copper dissolving into the cargo from the alloy.
Concentrations of copper in aviation kerosene fuel above 10 parts per billion (ppb) start to
affect thermal stability and 50 ppb invariably results in failure to meet specified requirements.
For this reason, aviation kerosene shall not be carried in ships fitted with heating coils made
from copper-containing alloys.
2.8 TANK COATINGS
2.8.1 Temperature restrictions
In ships with coated tanks, the temperature and pressure of washing water should not
normally exceed 66 °C and 10,5 kg/cm² respectively. However, these may be increased
subject to the following criteria:
Agreement from the coating manufacturer that excessive heat and/or pressure will not
damage the coating.
Agreement from the tank cleaning equipment manufacturer that excessive heat or pressure
will not cause damage to the machines.
The temperature of the washing water should always be at least 15 °C above the pour point
of the previous cargo.
In coated tanks of white oil carriers, washing with cold water is generally adequate, except
where more stringent cleaning is required after the carriage of vegetable oils, lubricating oils
and diesel fuel. Hot water (and/or detergents) may be used occasionally to degrease tank
structures, expedite gas-freeing for entry or where a gas-free condition is required for a major
change of grade. When hot water is used this should be in accordance with these criteria.
2.8.2 Coating compatibility
Although not directly related to tank washing, it should be noted that tank coatings are not
compatible with all products. Problems usually relate to chemicals rather than petroleum
products, but manufacturers' resistance lists (usually kept on board) should be consulted if
there are any doubts regarding coating compatibility.
Organic epoxy coatings can absorb some chemical cargoes, particularly chlorinated solvents.
The contamination potential to subsequent cargoes (particularly aviation kerosene) may
be considerable, as significant quantities can be absorbed and retained, depending on
the chemical, exposure time, temperature, specific coating type, thickness, condition, etc.
Contamination can persist after several subsequent cargoes and washings.
For aviation fuels, many oil companies have their own list of acceptable coatings. Cargo
tanks with zinc silicate coatings or zinc silicate linings should not be used for transportation
of jet fuel because of the potential adverse impact on fuel thermal stability. Where this is
unavoidable, specialist advice should be sought regarding additional testing requirements,
e.g. thermal stability testing at elevated temperatures prior to loading and discharge. The
charterer should be consulted regarding coating acceptability for aviation fuel cargoes.
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2.8.3 Stainless steel
Although stainless steel is compatible with most grades it is subject to attack by chlorinated
compounds. This is made worse by the presence of water. Also, some stainless steel grades
are subject to attack by sea water, so if a sea water wash is used in a stainless steel tank this
should be followed immediately by a fresh water rinse.
Note: Some shore-supplied 'fresh' water can contain sufficient chlorine to attack/discolour
stainless steel.
2.8.4 Coating condition
Damaged, flaking or blistering paint can increase hold-up of residues from previous cargoes,
and tanks with damaged coating should be avoided, particularly for critical cargoes such as
naphthas, light distillate feedstock and aviation kerosene.
2.9 CARGO LINES
2.9.1 General
Procedures for line washing should be contained in the vessel's cargo operations manual.
Careful visual inspection of the actual pump room and above-deck piping configuration
should be undertaken to identify any problem areas or 'dead ends' which will require special
attention.
MARPOL pumps and lines should be included in all draining, cleaning and washing operations,
which should be recorded in accordance with current MARPOL regulations.
2.9.2 Cargo compatibility
When loading more than one grade of cargo, it should be determined whether the grades
are compatible in both the liquid and vapour state.
Compatibility between cargoes is entirely dependent on their essential characteristics and

the quality specification of each grade. Pipeline admixture should be kept to a minimum at
all times as each admixture will result in some change in the quality of the loaded cargo.
Permissible admixture of one cargo by another is governed by the tolerance of quality
characteristics such as flashpoint, colour, sulfur content, viscosity, etc.
In general, admixtures may only be permitted for those loadings where wash code 1 is shown
in Table 1.
2.9.2.1 Liquid compatibility

If the grades are not compatible, each grade should be loaded through a separate system
with segregation provided by two valves or a blind.
Where different but compatible cargoes, such as two grades of crude, are loaded, single
valve segregation may be acceptable providing that the critical valves have been tested and
proved tight.
14
If two or more cargoes are compatible, loading should be carried out in sequence commencing
with the most critical cargo. Any admixing which may occur should not adversely affect the
quality of the second cargo to be loaded. Lines should be drained and/or stripped between
grades.
2.9.2.2 Vapour compatibility

Vapours from a volatile cargo such as gasoline can be taken up in diesel or gas oil cargoes
which share the same vent systems, or are under the same positive pressure of inert gas. If
vapour mixing can occur, each cargo should be loaded on a separate cargo and vent system
with vent system cross-over valves closed and tagged. If it is not possible to load using
separate vent systems then, when the ship design allows without impacting on latest SOLAS
regulations, individual tanks should be isolated from the system.
Interconnecting inert gas block valves should be closed and tagged and if vapour
contamination from slops is possible, slops should be isolated from the main inert gas line.
The oxygen content of isolated slop tanks should be monitored to ensure that it remains less
than 8 % by volume.
Note: Before any tank is isolated from the main venting system due consideration should
be given to meeting the SOLAS requirements and a formal risk assessment should be
conducted. The pressure in any tank segregated from the main venting system should be
carefully monitored to ensure that individual tank venting arrangements are adequate to
prevent formation of vacuum or a build-up of pressure.
2.9.3 Testing of cargo lines and valves
On each occasion a tank is gas-freed and opened for entry, every effort should be made to
pressure test the associated internal pipelines and valves. A brief inspection of coatings and
fittings should be undertaken at the same time. On no account should cargo be used to test
pipelines and valves. Only clean water should be used for this purpose.
2.10 TANK CLEANING
Table 1 provides guidelines for cleaning.
The table assumes that tanks are coated and in good condition. Where this is not the case
additional cleaning may be required depending on the cargo involved; typically, the addition
of gas-freeing, descaling and mopping where wash only is specified.
Stripping and draining following discharge or washing is assumed to be thorough, such that
any liquid ROB is confined to the pump well (if present). All associated lines (suction, deck
lines, and drop lines, etc.) are to be cleared and drained of all product or water.
Where washing is specified this includes deck lines, loading drop lines and cross-over lines.
The following of these guidelines does not necessarily mean that the tank(s) will be acceptable
for the next intended cargo. The Master is ultimately responsible for the cleanliness of
the tank(s) and should ensure that the end result meets the owner's/charterer's/shipper's
expectation.
Consideration may be given to substituting mopping by enhanced stripping and drying

where such facilities are available.
15
Note: The internal tank structure must be considered, as internal framing/ steam coils/ fixtures
and fittings may affect the quantity of water or previous cargo ROB and may not allow the
tank to be considered 'dry' even after additional stripping and drying.
2.11 COMMENTS ON INDIVIDUAL CARGOES (CARGO TYPES)
2.11.1 Naphthas and light distillate feedstocks (and/or – clean condensate, feedstocks,
straight run benzene, pentane, natural gasoline, straight run gasoline)
Naphtha and light distillate feedstocks should not be contaminated by lead and should not be
carried directly after cargoes that contained lead, e.g. aviation gasoline. Tank coating should
be in good condition as blistered or flaking tank coating can be a source of contamination
from the previous cargo.
Oxygenates can affect naphtha processing and washing is therefore required when loading
naphtha into tanks which have previously contained unleaded gasoline cargoes. Sea water
washing should be followed by a fresh water rinse to remove chlorides.
When loading after any cargo containing FAME a hot water wash may be needed to remove
residues. Cargoes are generally water- and colour-critical.
Heavier feedstocks can tolerate minor admixing of aviation kerosene, kerosene, solvents or
lighter feedstocks.
2.11.2 Aviation gasoline (and/or – avgas, aviation spirit) and aviation turbine gasoline,
wide cut jet fuel, JP4, Jet B)
These products may have a high lead content and are often dyed.
Uncoated tanks should be hot water washed and have any loose bottom scale removed
before loading.
Water cannot be tolerated and extreme care should be taken to ensure that tanks and lines
are drained before loading or discharging. Hand mopping is recommended. Products are also
sulfur-critical.
Detergents and saponifiers should not be used to prepare tanks for aviation gasoline cargoes
as residues can cause fixed haze in the fuel and harm fuel filters/coalescers.
Contamination of aviation gasoline with oxygenates (ethanol, MTBE, etc.) could lead
to specification issues. Thorough washing is required to ensure prevention of cross-
contamination and the proposed tank cleaning/flushing plan should be discussed and agreed
with the charterer.
To avoid contamination from FAME it is recommended to have three intermediate cargoes

with no FAME between FAME (B100) or any cargo with a FAME content greater than 15 %
(B15) and an aviation gasoline cargo.
When following cargoes with a FAME content of 5 % or less (B5 or below), a hot water wash,
including flushing of pumps and lines, followed by draining is recommended as a minimum.
16
When following cargoes with a FAME content of 15 % (B15) or less, but above B5, a hot water
wash, including flushing of pumps and lines, followed by draining is again recommended as
a minimum. However, tanks must be in good condition and washing needs to be particularly
stringent. A single intermediate cargo with no FAME content is suggested as an alternative,
followed by a hot water wash, including flushing of pumps and lines, and by draining.
The very low tolerance for FAME contamination requires extreme care during sampling. To
reduce the possibility of drawing unrepresentative samples, consideration should be given to
cleaning of standpipes and stilling wells as part of the tank cleaning regime when tanks have
previously held cargoes containing FAME.
2.11.3 Leaded motor gasoline (and/or – premium/regular motor spirit, motor gasoline,
mogas)
These products are often dyed and may contain surfactant additives.
Only minimal amounts of higher boiling point cargoes such as gas oil can be tolerated
in motor gasoline. Depending on the product specification, up to 0,1 % volume may be
tolerated. Where the product is close to specification limits a nil tolerance level will apply.
Products are also sulfur-critical.
Tanks will require washing when following cargoes of dyed gas oil or kerosene. Uncoated
tanks should be hot water washed and have loose bottom scale removed before loading.
2.11.4 Unleaded motor gasoline (and/or – unleaded motor spirit, regular unleaded,
premium unleaded, super unleaded, toluene, methyl tertiary butyl ether (MTBE),
reformate, alkylate, cracked spirit, ethanol, motor spirit/gasoline blending
components)
Thorough tank washing is required when following leaded products, dyed gas oil or kerosene.
Products are also sulfur-critical.
before loading.
2.11.5 Ultra low sulfur gasolines
In addition to the comments in 2.11.4, these cargoes have a typical maximum sulfur content
of 10 ppm (or possibly 50 ppm depending on location). If they are to be loaded into tanks or
through lines that have previously contained cargoes that had a greater sulfur content, care
should be taken to ensure that admixing is kept to a minimum.
These products are salt-water-critical as the high specifications will not allow sodium or
potassium. Fresh water washing and mopping may be specified.
17
2.11.6 Solvents (and/or – special boiling point solvents, rubber solvent, unleaded cleaning
spirit, white spirit)
These are volatile unleaded products.
Due to wide variations in specifications within grades, specific guidance should be sought on
the allowable levels of admixing with other solvents.
Solvents are frequently odour-critical which can be a particular problem after gas oil cargoes.
Common vapour lines should be considered for isolation for this reason.
No admixing with other types of product can be tolerated and these products should not be
carried after leaded cargoes.
before loading.
2.11.7 Aviation jet fuel (and/or – aviation kerosene, dual purpose kerosene, Jet, Jet-A1,
Avtur, ATK, JP5, JP8, synthetic jet fuel)
Products are unleaded and fairly volatile.
Aviation jet fuel cargoes shall not be loaded on maiden voyages or on first voyages after a
dry dock where modifications to cargo handling systems (tanks, pumps and lines) have taken
place, due to the high risk of contamination.
Products may contain relatively high levels of sulfur which could affect the quality of a
subsequent low sulfur cargo.
Aviation jet fuel should not be carried after leaded products.
Very tight specifications preclude admixing by other cargoes except undyed general purpose
kerosenes with no biological components.
Water cannot be tolerated and extreme care should be taken to ensure that tanks and lines
are drained before loading. Hand mopping is recommended.
Due to strict limitations on biological contamination it is recommended to have three

intermediate cargoes with no FAME between FAME (B100) or any cargo with a FAME content
greater than 15 % (B15) and a subsequent aviation jet fuel cargo, and special cleaning
instructions should be obtained.
When following cargoes with a FAME content of 5 % or less (B5 or below), a hot water wash,
including flushing of pumps and lines, followed by draining is recommended as a minimum.
When following cargoes with a FAME content of 15 % (B15) or less, but above B5, a hot water
wash, including flushing of pumps and lines, followed by draining is again recommended as
a minimum. However, tanks must be in good condition and washing needs to be particularly
stringent. A single intermediate cargo with no FAME content is suggested as an alternative,
followed by a hot water wash, including flushing of pumps and lines, and by draining.
The very low tolerance for FAME contamination requires extreme care during sampling. To
reduce the possibility of drawing unrepresentative samples, consideration should be given to
cleaning of standpipes and stilling wells as part of the tank cleaning regime when tanks have
previously held cargoes containing FAME. Where the FAME content of a previous cargo is not
known it should be assumed to be 15 %.
18
Other cargoes can have a deleterious effect on aviation kerosene product quality and
intermediate cargoes are recommended in these circumstances. Cleaning chemicals shall not
be used to prepare tanks for aviation kerosene cargoes as residues can cause fixed haze in
the fuel and harm aviation fuel filters.
In all cases salt contamination needs to be minimised after washing with sea water. A fresh
water rinse is recommended following sea water wash but thorough mopping may suffice.
2.11.8 Premium and regular kerosenes (and/or – kerosene feedstock, burning oil, stove
oil)
Products may contain relatively high levels of sulfur which could affect the quality of a
subsequent low sulfur cargo.
Flashpoint may be critical such that admixing with low flashpoint cargoes in tanks and lines
should be avoided.
Admixing of dyed kerosene with undyed kerosenes can result in the undyed cargo not
meeting colour specifications. Tanks which have carried dyed products will require washing
and mopping dry prior to loading undyed products.
Where dye is not a concern, these products will not require tanks to be mopped after water
washing unless following lube oil or light fuel oil.
Small amounts of gas oil may be tolerated (up to 0,1 % volume), subject to comments under
2.11.9.
2.11.9 Gas oil and automotive diesel fuel (and/or – automotive gas oil, automotive diesel
oil, DERV, extra light fuel oil, distillate marine diesel)
Some admixing with lighter distillate cargoes such as kerosene is acceptable, depending on
minimum flashpoint requirements for the individual cargo. However, flashpoint requirements
will preclude admixing with any naphtha, motor gasoline or other cargoes with low
flashpoints.
Water contamination is a problem leading to 'haze' in the product. This can produce a water
layer and subsequent corrosion in downstream storage. Sodium in any dissolved salt can lead
to damage to blades if the fuel is used for gas turbines. Care should therefore be taken to
ensure that water is removed from tanks, pumps and lines before loading. Uncoated tanks
should be hot water washed and have any loose bottom scale removed before loading.
The admixing of dyed gas oil with undyed gas oil can result in the undyed material not
meeting the colour specification and tanks which have carried dyed products will require
washing prior to loading undyed products.
Saponifiers and degreasers can have a negative effect on gas oil or automotive diesel fuel
quality and if these are used hot water washing is recommended to remove any traces.
Increasingly, diesel fuels for road transport are blends of FAME and conventional diesel fuel-
blended biodiesel. These blends may simply be referred to as diesel fuel, but the grade name
may indicate the percentage of FAME. Thus a B5 diesel fuel contains 5 % FAME and a B15
19
diesel fuel, 15 % FAME. Cleaning procedures vary with the percentage of FAME in the blend
so it is important that shippers determine the FAME content of diesel fuel cargoes. Where the
FAME content of a diesel fuel cargo is not known it should be assumed to be 15 %.
Gas oil blends with bio-gas oil are also becoming more common and the same precautions
should be applied to these products as for blended biodiesel.
Note 1: These comments also apply to FAME and other fatty acid esters.
Note 2: Some national specifications do not permit FAME in diesel which is not designated
as biodiesel, even at contamination levels. In such cases precautions similar to those used for
aviation jet fuel should be followed.
Note 3: Some gas oils may contain up to 2 000 ppm sulfur.
2.11.10 Ultra low sulfur automotive diesel fuel (and/or – ULSD, ULS turbine gas oil, LS marine
gas oil, ULS diesel)
In addition to the comments in 2.11.9 these cargoes typically have a maximum sulfur content
of 10 ppm (possibly 50 ppm depending on location). If they are to be loaded into tanks or
through lines that have previously contained cargoes that had a greater sulfur specification,
care should be taken to ensure that admixing is kept to a minimum.
These products are salt-water-critical as the specifications will not allow sodium or potassium.
Fresh water washing and mopping may be specified.
Flashpoint may be critical such that admixing with low flashpoint cargoes in tanks and lines
should be avoided.
2.11.11 Crude oil and condensate
The properties of crude oil cargoes vary considerably. General guidance, together with a list of
physical properties of many grades, together with washing and carriage recommendations,
is given in EI HM 40 Guidelines for the crude oil washing of ships' tanks and the heating of
crude oil being transported by sea.
Condensate which is dark in colour may be treated as crude oil. However some condensates
are 'clean', i.e. not heavily coloured, and may be of sufficient quality to allow loading of clean
products following a cold water wash, drain and mop (code 2M). However, clean condensate
may contain wax which will require additional cleaning. Quality certificates should always be
referenced for guidance.
When loading of aviation fuel is being considered, guidance should be sought from the cargo
owner and attention should be given to all parameters of the condensate, in particular:
a. ASTM D1500/IP 196 colour should be less than 2,5
b. ASTM D86/IP 123 distillation should be less than 10 % residue at 280 °C
c. Cloud point should be not greater than -10 °C
d. Viscosity at 20 °C should be less than 1,5 cst
20
2.11.12 Base lubricating oils
The quality of lubricating oils is greatly affected by admixing with water and tank preparation
will normally include mopping. Valves and strainers will also require opening and draining.
To maintain quality and avoid introduction of water, lubricating oils should be loaded, carried
and discharged under dry nitrogen and not dirty inert gas.
2.11.13 Vacuum gas oil (and/or – cracker feed, waxy distillate)
These cargoes are sodium-critical and tanks which have been salt water washed will require
fresh water washing to remove any salt traces. Vacuum gas oil may be loaded on top of some
light crude oils and condensates without washing. However, as with fuel oils, the need to
heat the product leads to a high flashpoint specification and precludes admixing with any
volatile residues.
2.11.14 Medium and heavy fuel oils
The admixing of these cargoes with waxy residues can result in the material not meeting the
maximum pour point specification limit. Tanks which have carried high pour point cargoes
should be carefully drained and stripped prior to loading.
The need to heat the product leads to a high flashpoint specification and precludes admixing
with any volatile residues. Washing will generally be required when loading these products
after crude oil cargoes.
2.11.15 Low sulfur fuel oil (and/or – low sulfur atmospheric residue (LSAR), low sulfur
waxy residue (LSWR))
In addition to comments in 2.11.14, these products are frequently traded with sulfur content
very close to the specified upper limit. Admixing with cargoes with higher sulfur content
should therefore be kept to a minimum. Hot washing may be required when loading after
crude oils or other fuel oils depending on the characteristics of the cargo discharged.
Cargoes for refinery cracking will also be sodium-critical and tanks which have been salt
water washed will require washing with fresh water to remove any salt traces.
2.11.16 Light fuel oil
The admixing of these cargoes with waxy residues can result in the material not meeting the
maximum viscosity and/or pour point specification limit. Tanks which have carried high pour
point or high viscosity fuel oil or crude oil should be hot washed at the highest permitted
temperature to remove wax traces. The need to heat the product leads to a high flashpoint
specification and precludes admixing with any volatile residues.
Washing may be avoided if a previous cargo of heavier grade fuel oil has low wax content
and ROB is minimal (less than 0,1 % of volume).
21
2.11.17 Gas to liquids (GTL) products
A number of GTL products are entering the market: typically naphtha, kerosenes and diesel.
Properties are as per similar non-GTL cargoes but all are low sulfur and low aromatic and
should be handled accordingly.
2.11.18 FAME and blended biodiesel
FAMEs vary considerably in properties, depending on the original source of the oil/fat.
However, all are prone to absorb water both from the atmosphere and from tank washing
activities. Tanks which have been subject to water washing should therefore be mopped dry
before loading any cargo of FAME or FAME/petroleum diesel blend.
2.11.19 Light cycle oil (LCO)
LCO can be a dark or clear, straw coloured product.
With regard to products following LCO: dark LCO should be treated as a black oil cargo and
clear LCO can be treated as gas oil.
Cleaning before loading LCO will depend on the end use of the product and, of course, the
previous cargo. Advice should be requested from the cargo owner/charterer.
22
Table 1: Cleaning recommendations
Grade discharged
blended >15 % FAME B15

recommendations of HM
Diesel blended with 5 %

Motor gasoline (leaded)
condensate (see note 6)

Ultra low sulfur gas oil/
containing oxygenates
Ultra low sulfur motor
Natural gasoline NGLS
up to5 % FAME (B5 or
to 15 % FAME (B15 or
only with the written
FAME or diesel/gas oil
Fuel oil (sulfur > 1 %)

(ethanol, MTBE, etc.)
or higher (see note 4)

This table to be used
Aviation jet fuel and
Diesel blended with

gasoline (unleaded)
Kerosene (un-dyed)
Naphtha (lead free)
Cargo to be loaded
Base lubricating oil

lower) (see note 4)
lower) (see note 4)
Low sulfur fuel oil

Aviation gasoline
Gas oil (un-dyed)

Aviation turbine
Kerosene (dyed)
Motor gasoline
Motor gasoline
Vacuum gas oil

Gas oil (dyed)
(sulfur < 1 %)
Crude oil and

components
White spirit
(unleaded)
Solvents
gasoline
50, see:
diesel
2.11.2 Aviation gasoline # 1 1 2 2 1 1 1 2M 2M 2M 2M 2M 2M 2M 3M 3M* X* 2M 2M X* X* X* X* X*
2.11.2 Aviation turbine gasoline # 2M 1 1 2M 2M 2M 2M 2M 2M 1 2M 1 2M 1 3M 3M* X* 2M 2M X* X* X* X* X*
2.11.7 Aviation jet fuel and 2M 2M 1 2M 2M 2M 2M 2M 2M 1 2M 1 2M 1 3M 3M* X* 2M 2M X* X* X* X* X*
components #
2.11.4 Motor gasoline (unleaded) 2M 1 1 1 1 1 2M 1 1 1 1 1 2M 1 1 1 2M 2 2 3M 3M X X X
containing oxygenates
23
(ethanol, MTBE, etc.)

2.11.4 Motor gasoline (unleaded) † 2 1 1 1 1 1 2 1 1 1 1 1 2 1 1 1 2 2 2 3 3 X X X
2.11.5 Ultra low sulfur motor 2M 2M 2M 2M 2M 1 2M 2M 2M 1 (see 2M 1 (see 2M 1 1 1 2 3M 3M X X X 3M X
gasoline (unleaded) † note 5) note 5)
2.11.3 Motor gasoline (leaded) † 1 1 1 1 1 1 1 1 1 1 1 1 2 1 1 1 2 1 1 3 3 X 3 X

2.11.1 Naphtha (lead free) †# X 1 1 2 1 1 X 1 1 1 1 1 1 1 2 2 3 1 1 3 3 3 3 X
2.11.1 Natural gasoline (NGLs) † X 1 1 1 1 1 X 1 1 1 1 1 1 1 1 1 2 1 1 1 3 3 3 X
2.11.8 Kerosene (un-dyed) 2P 2P 1 2P 2P 2P 2P 2P 2P 1 2 1 2 1 1 1 2 1 2 2 X X 3 X
2.11.8 Kerosene (dyed) 2P 2P 1 2P 2P 2P 2P 2P 2P 1 1 1 1 1 1 1 2 1 2 2 X X 3 X
2.11.9 Gas oil (un-dyed) 2P 2P 1 2P 2P 2P 2P 2P 2P 1 2 1 2 1 1 1 2 1 2 1 3 3 3 3P
2.11.9 Gas oil (dyed) 2P 2P 1 2P 2P 2P 2P 2P 2P 1 1 1 1 1 1 1 2 1 2 1 3 3 3 3P
2.11.10 Ultra low sulfur gas oil/diesel 2M 2M 2M 2M 2M 2M 2M 2M 2M 1 (see 2M 1 (see 2M 1 1 1 2 3M 3M X X X 3M X
note 5) note 5)
2.11.6 Solvents †# and white spirit 2M 2M 2M 2M 2M 2M 2M 2M 2M 2M 2M 2M 2M 2M 2M 2M 2M 2 2 X 3M X 3M X

2.11.11 Base lubricating oil 2M 2M 1 2M 2M 2M 2M 2M 2M 1 1 1 1 1 1 1 1 3M 3M LU X X X X
2.11.13 Vacuum gas oil # 2P 2P 1 2P 2P 2P 2P 2P 2P 1 1 1 1 1 1 1 1 2P 2P 1 1 1 1 3P
2.11.14 Fuel oil (sulfur > 1 %) 2P 2P 1 2P 2P 2P 2P 2P 2P 1 1 1 1 1 1 1 1 2P 2P 1 1 1 1 3P
2.11.15 Low sulfur fuel oil 2P 2P 1 2P 2P 2P 2P 2P 2P 1 1 1 1 1 1 1 1 2P 2P 1 3 3 1 3P
(sulfur < 1 %)
2.11.11 Crude oil, condensate † 2 1 1 1 1 1 2 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
Table 1: Cleaning recommendations continued
Key:
Code Cleaning recommendations

X Not to be loaded without special cleaning instructions.
X* Not to be loaded without special cleaning instructions. Three clean and zero biological content intermediate cargoes recommended.
1 Drain tanks, lines and pumps well. If previous cargo shows signs of instability or oxidation (dark colouring or broken down from sediment)
then use code 2M.
2 Wash with cold water and drain well.
3 Wash with hot water and drain well.
3M* A stringent hot water wash, drain and mop may be sufficient if tanks are in good condition. As an alternative one clean product/zero
biological content intermediate cargo is recommended, followed by hot water wash, drain and mop. Fresh water rinse required if sea
water is used. Consideration may be given to substituing mopping by enhanced stripping and drying, see 2.10.
P Purge to below 2 % hydrocarbon by volume.
M Gas free, lift scale and mop. Consideration may be given to substituting mopping by enhanced stripping and drying, see 2.10.
24
# Fresh water rinse after any salt water wash when loading these products.
LU Reduced cleaning may be permitted depending on lubricating oil specification. Otherwise apply code 3M.
Notes 1. Additional cleaning may be required for uncoated tanks, tanks with extensive coating breakdown or where specified in the charter
party.
2. † Benzene may be present in any petroleum product but may be present in higher concentrations in those products marked †. Refer to
ISGOTT for precautions in handling cargo suspected of having a benzene content and prior to entering a space which has contained
such a cargo.
3. In cases where the FAME content in diesel is unknown, and in locations where reporting of FAME content is not required, it shall be
assumed to be 15 %.
4. Comments regarding FAME also apply to FAEE and other fatty acid esters.
5. Where high sulfur kerosene or gas oil has been discharged Code 2 should be used.
6. Refer to quality certifcate: some condensates are of sufficient quality to allow loading of clean products, including aviation fuel,
following cleaning to code 2M
7. Lubricating oil should be loaded, carried and discharged under air or nitrogen only.
ANNEX A
GLOSSARY OF TERMS
For the purposes of these EI guidelines, the terms used should be understood to have the
following meanings:
admixture; transmix Quantity of a different product (usually from a previous batch

or cargo) which becomes mixed with the current batch or
cargo.
ATK Aviation turbine kerosene.
aviation jet fuel:

conventional Hydrocarbons for use in aviation turbine engines and derived
from the following conventional sources: crude oil, natural
gas, liquid condensate, heavy oil, shale oil and oil sands.
synthetic Hydrocarbons for use in aviation turbine engines and
derived from alternative sources such as coal, natural gas,
biomass and hydrogenated fats and oil by processes such as
gasification, Fisher-Tropsch synthesis and hydroprocessing.
ballast Water taken on board when a vessel is empty or partially
loaded/discharged to increase draught so that the propeller is
fully immersed, stability and trim are maintained, and stresses
minimised.
clean ballast Ballast contained in cargo tanks that have been COW’d
(where appropriate) and thoroughly water washed. It may be
discharged to sea and meets MARPOL requirements.
black oils Petroleum products containing residual components which
make them dark in colour.
blended biodiesel Diesel fuel which is a blend of biologically-derived
components (e.g. FAME, FAEE or other fatty acid esters), and
petroleum diesel. The percentage of biological component is
often designated in the grade name, e.g. B15 indicates 15 %
biological component.
blended bio-gas oil Gas oil which is a blend of biologically-derived components

(e.g. FAME, FAEE or other fatty acid esters), and petroleum
gas oil.
bottom wash Washing operations restricted to the lower parts of the tank
bulkheads, internal structures and bottom of tanks. This can
only be carried out by vessels equipped with programmable
tank washing machines.
clingage Material which adheres to the surfaces of tank walls and
structures, both horizontal and vertical, within empty and part
empty tanks, other than bottom surfaces.
25
crude oil washing The use of a high pressure stream of the crude oil cargo
(COW) to dislodge or dissolve clingage and sediments from the
bulkheads, bottom, and internal tank structures of a vessel
during the discharge operation.
fatty acid ethyl ester Sometimes referred to as biodiesel or B100 (not yet widely
(FAEE) used but properties similar to FAME).
fatty acid methyl Sometimes referred to as biodiesel or B100.

ester (FAME)
flashpoint Lowest temperature of the test portion, corrected to a
barometric pressure of 101,3 kPa, at which the application
of an ignition source causes the vapour of the test portion to
ignite and the flame to propagate across the surface of the
liquid under the specified conditions of test.
full cycle washing Washing operation in which the complete cargo tank is
washed, either by programmable or non-programmable
machines.
gas-free A tank, compartment or container is gas-free when sufficient
fresh air has been introduced into it to lower the level of any
flammable, toxic, or inert gas to that required for a specific
purpose, e.g. hot work, entry, etc.
IMO International Maritime Organization.
inert gas (IG) a gas or gas mixture used to render the vapour space in the
cargo tank non-flammable.
ISGINTT International Safety Guide for Inland Navigation Tank-barges
and Terminals.
ISGOTT International Safety Guide for Oil Tankers and Terminals.
ISO International Organization for Standardization.
MARPOL Latest version of the Protocol of 1978 relating to the

International Convention for the Prevention of Pollution from
Ships, 1973.
oxygenate An oxygen containing organic compound such as an alcohol
(e.g. ethanol), or ether (e.g. MTBE, ETBE) that can be used as
a gasoline component.
persistent oil The International Oil Pollution Compensation (IOPC) Fund
guidelines consider an oil as non-persistent if, at time of
shipment, at least 50 % of the hydrocarbon fractions, by
volume, distil at a temperature of 340 ºC and at least 95 % of
the hydrocarbon fractions, by volume, distil at a temperature
of 370 ºC when tested in accordance with ASTM D86. A
persistent oil is one which does not meet these criteria.
26
pour point The lowest temperature at which a sample of petroleum

product will continue to flow when it is cooled under
specified standard conditions (see IP 15/ASTM D 97).
purging The introduction of inert gas into a tank already in an inert
condition with the object of further reducing the existing
oxygen content and/or the existing gas content to a level
below which combustion cannot be supported if air is
subsequently introduced into a tank.
remaining on board Sum of measured liquid volume, including free water, and
(ROB) measured non-liquid volume but excluding vapours, in cargo
tanks on completion of discharge.
saponifier A solution of organic or inorganic bases (alkalines, e.g.
caustic soda), and various agents, such as wetting agents and
dispersants, which react with, and promote the removal of,
non-water-soluble contaminants, such as vegetable oils.
segregated ballast Vessels having sufficient dedicated ballast tanks to enable safe
tankers (SBTs) seagoing operations under normal weather conditions. See
also heavy weather ballast.
slop tank(s) For the purposes of these guidelines tank(s) utilised as a

reservoir for COW medium and receipt of tank washings.
SOLAS International convention for the safety of life at sea
stripping The removal of the final contents of a cargo tank, possibly
using equipment additional to the main cargo pumps.
trim The difference between the fore and aft draught of the
vessel. When the aft draught is greater than the forward
draught, the vessel is said to be trimmed 'by the stern'. When
the aft draught is less than the forward draught, the vessel is
said to be trimmed 'by the head'.
true vapour pressure The absolute pressure exerted by the gas produced by
(TVP) evaporation from a liquid, when the gas and liquid are in
equilibrium at the prevailing temperature.
viscosity A measurement of a fluid’s resistance to flow at a prescribed
temperature. In this document the unit of Kinematic Viscosity,
the centistoke (cSt) has been used which is equivalent to
mm²/s.
wax A mixture of long chain hydrocarbons that crystallise at
different temperatures as the overall fluid temperature falls.
white oils Clean, refined petroleum products which are not dark in
colour such as motor spirit, kerosene, gas oil, diesel fuel and
blending components.
27
ANNEX B
REFERENCES
The following standards and papers have been used in the preparation of this publication:
Central Commission for Navigation on the Rhine (CCNR) – http://www.eda.admin.

ch/smno/en/home/zentralkommission-fuer-die-rheinschifffahrt.html
Oil Companies International Marine Forum (OCIMF) – https://www.ocimf.org

International safety guide for inland navigation tank-barges and terminals
Energy Institute (EI) – https://www.energyinst.org

EI/JIG 1530 Quality assurance requirements for the manufacture, storage and distribution of
aviation fuels to airports
HM 40 Guidelines for the crude oil washing of ships’ tanks and the heating of crude oil being
transported by sea
International Maritime Organization (IMO) – https://www.imo.org

Crude oil washing systems, revised 1983
International convention for the safety of life at sea (SOLAS), 1974, including amendments,
Chapters 11 and 12
Regulations for the prevention of pollution by oil, Annex 1 and Annex II of MARPOL 73/78
including amendments
Witherbys – http://www.witherbys.com
International safety guide for oil tankers and terminals, 5th edition
28
This publication has been produced as a result of
work carried out within the Technical Team of the
Energy Institute (EI), funded by the EI’s Technical
Partners and other stakeholders. The EI’s Technical
Work Programme provides industry with cost
effective, value adding knowledge on key current
and future issues affecting those operating in the
Energy Institute energy industry.
61 New Cavendish Street
London W1G 7AR, UK
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ISBN 978 0 85293 982 6

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Hydrocarbon management

Guidelines for the cleaning of tanks

The EI is licensed by:

For further information, please visit http://www.energyinst.org

Apache North Sea Repsol Sinopec

Copyright © 2017 by the Energy Institute, London.

ISBN 978 0 85293 982 6

Published by the Energy Institute

1 Introduction and scope . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5

2 Tank cleaning guidelines . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6

2.11.1 Naphthas and light distillate feedstocks (and/or – clean condensate

Table 1 Cleaning recommendations . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 23

Annex A Glossary of terms . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 25

Technical Department, Hydrocarbon Management

Bazan Group (Oil Refinieries Limited)

The guidelines were compiled by Melverley Consultants Limited.

1 INTRODUCTION AND SCOPE

Nothing in the guidance contained in these guidelines suggests or encourages deviation

2 TANK CLEANING GUIDELINES

2.1 GENERAL INFORMATION

2.1.1 Introduction and cleanliness standards

Tank cleaning is carried out to:

It can be accomplished by means of portable or fixed tank washing machines, or sometimes

In order to reduce unnecessary bunker consumption, impact on the environment and

2.1.2 Inert gas

2.1.3 Static electricity

2.2 BOTTOM AND LINE FLUSHING

2.2.2 Fuel oil cargoes

2.3 ELIMINATION OF WATER FOR CRITICAL CARGOES

2.4 DISPOSAL OF RESIDUES

2.4.1 Cargo residues

2.4.2 Scale and solid residues

2.5 TANK WASHING

2.5.2 After black oil cargoes

2.5.3 After white oil/clean product cargoes

2.5.4 After crude oil cargoes

2.5.5 After vegetable oil cargoes

Vegetable oils can be defined as drying, non-drying and semi-drying.

Semi-drying oils have iodine values between 110 and 140.

Contamination of aviation kerosene with FAME is a serious concern. Intermediate cargoes

2.5.7 After gasoline/ethanol blended cargoes

2.5.8 Use of chemicals

Due to environmental considerations, tank cleaning chemicals should no longer be used

2.5.9 Cleaning of sampling equipment and stilling wells

2.6 TANK INSPECTIONS

2.6.2 Inerted tanks

Reference should be made to ISGOTT recommendations with regard to inerting.

2.7 HEATING COILS

2.7.2 Heating coils made from copper-containing alloys

2.8 TANK COATINGS

2.8.1 Temperature restrictions

2.8.2 Coating compatibility

2.8.3 Stainless steel

2.8.4 Coating condition

2.9 CARGO LINES

2.9.2 Cargo compatibility

Compatibility between cargoes is entirely dependent on their essential characteristics and

2.9.2.1 Liquid compatibility

2.9.2.2 Vapour compatibility