SCAA+Member+ Driven+Research+Coffee+Staling+Report
SCAA+Member+ Driven+Research+Coffee+Staling+Report
I
n food science, coffee is known as a shelf stable product. This is because unlike many other food products, it does
not spoil due to enzymatic or microbial processes (Nicoli and others 1993; Illy and Viani 2005; Anese and others
2006). However, the specialty coffee industry recognizes the importance of chemical reactions and physical
changes that occur after roasting, and are aware that some of these changes are responsible for staling (Nicoli and
others 2009). The staling rate of coffee can be defined as the perceptible amount of negative flavor change over a
given amount of time. This rate can be utilized to determine a shelf life for roasted coffee. Shelf life is an individual
set point that must be based on individual company best practices. Because coffee does not spoil, shelf life best
practices must be based on a loss of quality measured by sensory methods. However, capturing the exact nature,
quantity, and rate of staling is inherently challenging due to both the diversity of flavors possible in the bean itself
and to the volatility of delicious flavor and aroma compounds that contribute to the ephemeral nature of roasted
coffee.
Defining the science behind staling is problematic. The chemical and physical changes that occur in coffee
after roasting make experimental control, repeatability, and data analysis all but impossible. Staling occurs in two
simultaneous ways over time: the loss of fresh flavors and the formation of “off” flavors. There is adequate evidence
that oxygen is the primary enemy of roasted coffee, followed closely by temperature and moisture (Cappuccio and
others 2001; Cardelli and Labuza 2001; Anese et al. 2006). Secondary staling factors include things that influence
how coffee interacts with the external environment, including roast, coffee porosity, surface area/grind, light
exposure, and water activity. For more about the science of coffee staling, see the SCAA Literature review on the
shelf life of roasted coffee, available on the SCAA Digital Chronicle.
It is the mission of the Specialty Coffee Association of America (SCAA) to recognize, develop, and promote
specialty coffee. Specialty coffee should always taste as delicious as possible. Maintaining the freshness of coffee
is critical to preserving taste, especially as coffee is often sent home with customers. This fact led the SCAA to
acknowledge a need for sensory testing within the coffee industry as with customers. This work was conducted as a
joint effort between the SCAA and the Roasters Guild due to interest expressed by the membership. Together, the
groups focused on answering some fundamental, taste-based questions. The industry has many assumptions about
what happens to the taste of roasted coffee over time. A group of Roasters Guild-based project leaders set out to
validate some of those assumptions and learn more about how production choices can influence the taste of coffee.
Based on what is already known about the staling of coffee (see the SCAA Chronicle Literature Review on this
topic) and the above research questions, four simple yet important hypotheses were formed:
1. The older the coffee, the more flavor is lost and tasters will like the coffee less.
2. Packaging type affects the staling rate of specialty coffee. Packaging with protection against oxygen,
moisture, and heat will delay staling for longer than less protective packaging.
3. Different coffees (including variations in cultivar, origin, and processing method, among other factors)
will lose flavor differently over time.
4. Coffee that is rested before packaging will have lower cupping scores and will afterward stale at the
same rate as non-rested coffees, having lost many volatiles and flavor compounds during prolonged
exposure to air.
Treatment of Coffees. Three coffees were obtained by Dillanos Coffee Roasters for this project; one from Colombia, Rwanda, and
Brazil. These coffees were chosen for their contrasting origins and cup profiles in order to highlight differences for the sub-experiment
to investigate whether different coffees stale differently. The coffee from Colombia was chosen as the primary experimental coffee due
to its characteristic washed, mild cup profile. It was utilized in the packaging-type and resting-time experiments. See Table 1 for more
specific information about each coffee.
Finca Potosi,
Fazenda Sertao, Abakundawa Coop,
Farm/Location Valle del Cauca,
Carmo de Minas Musasa
Caicedonia
Figure 1. Roast curves [temperature in degrees Fahrenheit (°F) in roaster over time]
for each roast of the primary experimental coffee from Colombia.
Experiments. For this member-driven initiative, one primary experiment and two sub-experiments were designed and conducted to
test the hypotheses listed above. All of these experiments involved experienced cuppers, one was conducted with specialty coffee
customers in SCAA-member retail locations, as well as with specialty coffee professionals at the 2012 Roasters Guild Retreat. The
primary experiment involved all three groups of people and attempted to address research questions and hypotheses one and two,
listed above, which have to do with the staling of roasted coffee in different packaging conditions. Research questions and hypotheses
two and three were addressed as sub-experiments, as they were conducted on a smaller scale and served as supporting information to
primary objective, specifically to investigate the effect of different coffees and resting-times on coffee staling. See further clarification
of these experiments in Table 4 and narrative explanations in below paragraphs.
Experienced
Cuppers;
85; 103;
1 & 2: Coffee Staling by Specialty Coffee
Primary Colombia and 77,
Packaging Type Customers;
respectively
and RG Retreat
Participants
Colombia,
Experienced
Sub-Experiment #1 3: Different Coffees Rwanda, and 80
Cuppers
Brazil
Experienced
Sub-Experiment #2 4: Resting Times Colombia 76
Cuppers
An experienced cupper was defined for purposes of these experiments as “one who cups three or more times per week and scores
coffee based on the SCAA form.” The SCAA recruited members to participate through newsletters, social media (Facebook and
Twitter), individual outreach, and Roasters Guild emails. Members were asked to self-report whether they fit into the experienced
cupper category and were trusted to only include colleagues that also fit into this category. Many members expressed interest in
helping out, and in the end 85 experienced cuppers from over 60 SCAA member companies participated. For the experiment at
Roasters Guild Retreat, 78 coffee professionals participated by completely filling out SCAA cupping forms. For customer experiments
facilitated by SCAA member companies, over 100 specialty coffee customers participated at 15 different retail locations.
Storage and Distribution. After roasting and packaging, the coffees were all stored together until shipment to SCAA-member
volunteer participants on June 15, 2012. In the case of coffees cupped at Roasters Guild Retreat, they were stored at Dillanos Coffee
Roasters until ground transport to the event on August 17, 2012. Prior to shipment, all coffees were stored in a climate-controlled
building in cabinets and boxes in a single room with no outside-facing windows. Coffee was distributed to member volunteers in order
to distribute the sub-experiments among participants and were labeled with codes to prevent biased responses. Packages of coffee
and instructions were shipped via ground or air depending on the distance from Washington State, to minimize shipping time (see
Figure 2). Shipping was generously sponsored by Cablevey Conveyors.
Primary Experiment: Coffee Staling by Packaging Type. For this experiment, three common methods of packaging were chosen to
represent the majority of packaging categories utilized by Roasters Guild members: a natural kraft paper bag; a foil bag with a one-
way valve; and a foil bag with a one-way valve, flushed with nitrogen gas. The kraft bags were of one-pound size, with a tin-tie closure
and a polypropylene liner. This liner is produced by the manufacturer to keep coffee oils from wicking onto the paper outer and is not
an effective barrier to oxygen. Kraft bags are described by the manufacturer as “designed for products that do not require long shelf
life.” The foil bags were also a one-pound size. The bags have three-ply polyester and aluminum lamination, providing an oxygen and
moisture barrier. These bags are gusseted with a one-way valve. Nitrogen-flushed foil bags were the same composition as the one-
pound foil bags, but were a five-pound size. This size difference did not change any potential comparison as nitrogen flushing removed
almost all oxygen within them. Each bag type was coded with a number and letter descriptive of the specific treatment of coffee inside.
This code was unrecognizable to cupping leaders. Coffees in kraft and foil bags were sent to 30 locations for customer cuppings and
over 100 customer rankings were returned to the SCAA for analysis. After the return of all experienced cupper scoring forms there
were at least 124 individual cupping results for the foil and kraft bag types. The number scores returned for coffee packaged foil N
flushed bags was lower than expected and therefore was focused on during the Roasters Guild Retreat event. All three packaging
types were also used during the Roasters Guild Retreat coffee professionals cupping.
Customers were given two groups of three coffees of various ages, bagged in both foil and kraft packaging types, and asked
to rank them in order of preference. They were also able to add tasting notes. They were not instructed to rank a particular attribute,
but to simply rank the coffees in order of their own personal preference. The two groups of coffees were presented to them in random
arrangements so that rankings could be converted to a scale of six. These rankings were then averaged by bag type and days after roast
to help understand customer preference between packaging types over time. Although this method was very simple it was deemed
adequate for the scope of this study, which was essentially pilot-level for consumers and will likely be expanded upon in subsequent
SCAA experiments.
Sub-Experiment #1: Different Coffees. For this sub-experiment, experienced cuppers scored three different coffees (from Colombia,
Brazil, and Rwanda) of differing ages in one packaging type (foil bag), bagged immediately after cooling (no resting time). These coffees
were distributed to participants in order to facilitate an even number of the different coffees tasted/sample size, as no one cupper
could cup the full set of experimental coffees (five roast days x three coffees = 15 coffees). Coffees for this experiment were sent to 20
member locations for group cuppings. They were tasted by experienced cuppers using the SCAA cupping protocol and cupping form,
which was returned to the SCAA for analysis. A minimum of 79 individual cupping scores were collected for each of the three coffees
packaged in the foil bag after no resting time.
Sub-Experiment #2: Resting-Time. Four different resting times (including a control of no resting time) were chosen to reflect typical
roasting practices. Resting times tested were: 0 hours (after cooling to room temperature), 12 hours after roast, 24 hours after roast,
and 48 hours after roast. The Colombian coffee was rested in buckets open to the air in the roastery to simulate typical small roaster
practices. Experienced cuppers evaluated rested coffee of different ages. Again, no one cupper was able to evaluate the full set of
coffees (five roast days X four resting times = 20 coffees), therefore partial sets were distributed randomly to cuppers in order to
facilitate even sample sizes among treatments. Coffee from this experiment was sent to 20 locations. At least 75 individual cupping
forms were collected from each of the four resting-time treatments.
Data Analysis and Statistics. Data were compiled and analyzed by the SCAA Coffee Science Manager. Coffee roast levels were tested
for differences with an analysis of variance (ANOVA) test. Each cupper was assigned a number to track all coffees that they cupped.
For the purposes of this experiment, only “total coffee score” on the SCAA cupping form was used to evaluate coffees. Descriptive
statistics were run on experienced cupper scores and customer rankings based on days after roast and packaging type.
Cupping dates were grouped by week to evenly distribute results by days after roast. Both experienced cupper scores
and customer rankings were tested for differences using an ANOVA test by weeks after roast and packaging type. Differences in
experienced cupper scores (also grouped by week) on coffee type and resting times were tested for significance with ANOVA tests.
Figure 3. Regression analysis on total cupping scores by roast level (Agtron score).
Regression analysis indicated that the roast level of coffees had no effect on score (R2=0.002).
Primary Experiment: Coffee Staling by Packaging Type. Experienced cuppers scored Colombian coffee of a variety of ages (days
after roast) packed in three different bag types to estimate the effect of staling over time. However, due to a small number of scores
returned on coffee packaged in foil N flushed bags, this data was excluded from experienced cuppers (see Figure 5). When looking at
days after roast, there was large variance in coffee scores. Regression analyses were run on both packaging types and were not robust
(R2=0.06 and R2=0.01 for kraft and foil bags, respectively). Despite the variation seen in cupping scores, the slopes of these regressions
were different from one another, indicating that the staling rates for these bag types were likely different. The ANCOVA statistical test
confirmed that the packaging types likely resulted in different rates of staling, with coffee in kraft paper bags staling faster than coffee
in foil valve bags (p=0.04). This trend was nicely demonstrated when cupping scores were averaged (see Figure 6). Slopes representing
the decline of cupping scores over time are clearly steeper, indicating faster loss of flavor for kraft paper bags relative to foil valve bags.
Staling rates were not calculated in rise-over-run (loss of score over time), as these rates were not expected to be exact (as evidenced
by regression analyses) or applicable to all coffees (as evidenced by results of the coffee sub-experiment). However, the results
indicating different staling rates were encouraging and warrant further research on this topic.
Figure 7. Averaged scores from specialty coffee professionals of the Colombian coffee, bagged immediately after cooling in either foil (filled
dots), kraft (open dots), or nitrogen-flushed (filled triangles) bags, with standard errors. Lines demonstrate the differing slopes, representing
the decline of coffee scores over time (i.e., staling rates).
Specialty coffee customers ranked the Colombian coffee of different ages and packaging types, based on overall preference.
When all rankings were examined, customers did not show preference based on time after roast. This indicates that perhaps as a group
they were unable to differentiate between freshly roasted versus older coffees (see Figure 8). Regression statistics were run relating
days after roast to ranking and these were not significant (Both R2s <0.001). Also, the slopes of these regressions were not different
than each other (ANCOVA test, p=0.39). However, customers trended toward preferring coffees packaged in foil bags and this was
most apparent when rankings were averaged (see Figure 8). This trend was found to be statistically significant when coffee age was not
considered (ANOVA test, p=0.04; see Figure 9).
Figure 9. Averaged customer ranking (scale of 1-6, where 1 is most preferred) demonstrating that customers prefer coffee in foil bags (filled
circles) more than kraft bags (open circles). This trend was statistically significant when data from all days after roast were grouped (p=0.04).
Figure 4. The individual scores of coffees from Colombia (brown circles), Brazil (blue triangles), and Rwanda (yellow squares) as they aged
(days after roast), as measured by experienced cuppers. Regression analysis results for coffees from Colombia (solid line), Brazil (dashed
line), and Rwanda (dotted line) are plotted on top of individual results for each coffee.
It is the assumption of much of the coffee industry that different coffees stale at different rates due to their unique chemical
and physical properties. As this had not been tested within the specialty coffee community, it was a necessary research question for
this group to address. The hypothesis that different coffees would stale differently was found to be true in some but not all cases.
Different coffees did stale at different rates in this particular bag type (foil). It is important to note that there was no attempt to break
out all of the possible mechanisms contributing to these differences. At this juncture, we cannot speculate about the specific reasons
that these particular coffees had different staling rates. However, in subsequent experiments it will be important to remember that
coffees of different varieties, from different origins, or differently processed are likely have a suite of chemical differences that not only
influences the way they taste, but also how they age and stale.
Sub-Experiment #2: Resting-Time. Experienced cuppers scored coffees that were rested for different amounts of time before being
packaged in foil bags. As with the other experiments, there was much variation in coffee scores at each day after roast. Regression
statistics were run on coffee scores for days after roast and were not significant. However, the slopes of these regressions differed a
great amount from each other, with coffees that had no resting time showing the slowest decline in score over time as compared with
rested coffees (see Figure 10). The staling rates (loss of cupping score over time) of all coffees rested before being packaged were found
to be statistically the same (ANCOVA, p=0.96) regardless of whether the coffee was rested for a short or long time. However, coffee that
was immediately packaged after cooling had a different slope (ANCOVA, p=0.04) that was less steep than the slope for rested coffees.
This indicates that non-rested coffee lost flavor (indicated by cupping score) at a slower rate than coffee rested before packaging,
perhaps because fewer volatile compounds were lost before the coffee was protected.
Figure 10. Experienced cupper scores and regressions for the Colombian coffee packaged in foil bags immediately after cooling (i.e., no rest;
brown circles, solid line) or rested in open buckets for 12 (blue circles, medium dashed line), 24 (yellow triangles, large dashed line), or 48
hours (green triangles, dotted line).
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