ALS Minerals Service Schedule AUD
ALS Minerals Service Schedule AUD
ALS Minerals Service Schedule AUD
www.alsglobal.com
ALS is pleased to announce the acquisition of Ammtec, a leading metallurgical and mineral testing consultancy with global recognition.
Established in 1979 and initially operating within the iron ore sector, Ammtec has since expanded its range of services as well as its commodity testing base. Services include: Bacterial leaching Comminution Cyanide detoxification Floatation Mineralogy Pressure acid leach PSI Ion Exchange resins Resin ion exchange SAG mill design SMC testing Solvent Extraction Pilot plant design and operation
The acquisition of Ammtec brings a depth of experience and knowledge which extends across the globe, for all mineral commodities and is complimented with world class analytical capability. Ammtec and ALS have similar business philosophies founded on the basic principles of providing the best quality service, accurate and timely delivery of results and a highly professional approach to business and problem solving. This alignment of core values ensures that you will continue to receive service of the highest standard.
TAbLE Of CONTENTS
Quality Assurance ..........................................................................................................3 Webtrieve ...................................................................................................................3 Sample Preparation .......................................................................................................4
Sample Submission ................................................................................................................................................ 4 Sample Preparation Packages ............................................................................................................................... 5 Individual Sample Preparation Procedures .......................................................................................................... 6 Specific Gravity & Bulk Density ............................................................................................................................. 7
Other Services..............................................................................................................36
Drill Core Services ................................................................................................................................................. 36 Mobile Sample Preparation Facilities .................................................................................................................. 38 Mine Site Laboratories.......................................................................................................................................... 39
www.alsglobal.com
ALS Minerals is the leading full-service provider of analytical geochemistry services to the Mining Industry the world over. Our integrated network of over 60 laboratories around the world ensures consistent quality and dependable client service wherever we might meet you. Our services are available through any one of the many general service laboratories listed on the back page of this schedule. However, we also provide custom services for on-site laboratory and sample preparation facilities as well as mobile laboratories and sample preparation installations. Consistent quality standards that can be continually tested and proven are essential to provide the secure knowledge that shareholders are given accurate information as a new resource is developed. Our analytical laboratory processes are controlled and constantly monitored in real-time so you can be sure of the integrity of your results. Our analytical laboratories in each region are also certified and registered with appropriate independent quality organizations. Our global network is linked together for our clients using our industry-leading Webtrieve system which allows you to see location and status data for your samples as well as access your data and review quality information. This edition of our Schedule of Services and Fees describes a broad selection of our global services but it is by no means a comprehensive list. For specific questions please contact our client services team or the lab nearest to you and we will be glad to help. Prices listed here do not contain locally applicable taxes. ALS Minerals reserves the right to alter listed prices at any time.
ALS Minerals is a division of ALS Group, providing services to the coal, environmental, food & pharmaceutical, industrial and petroleum industries. ALS Group is a wholly owned subsidiary of Campbell Brothers Limited, a publicly listed Australian Company (ASX code CPB).
ISO 9001:2008 registration & ISO 17025 accredited methods in North America
www.alsglobal.com
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Our custom LIMS (Laboratory Information Management System) has been designed to enhance laboratory quality assurance protocols and to provide traceability necessary for todays stringent reporting requirements.
A world class quality management system combines a program of honest and transparent internal monitoring with a program of external laboratory accreditation and certification. ALS Minerals Webtrieve system allows transparent access to laboratory quality performance for our managers and clients alike. Our laboratories on each continent are accredited to ISO/IEC 17025:2005 standards to provide complete assurance regarding quality performance in every aspect of our network. Accreditations are being continuously expanded and now apply to our Reno and Val dOr regional laboratories. Of course, all ALS Minerals operations, accredited or not, employ exactly the same operating and quality performance processes and all follow the best practice guidelines required for qualification under ISO standards. This year our standard QC protocols have been expanded to include monitoring of sample preparation duplicates. Using Webtrieve, it is now possible to review the performance of these duplicates for your project and the specific contribution that the preparation and analytical processes have made to analytical variance in your dataset.
Webtrieve
Webtrieve continues to be a key part of ALS Minerals services. Data retrieval, job progress, along with unprecedented access to laboratory details continues to be a standard part of the service. As services expand into new areas, Webtrieve functionality expands. Core cutting and core photography are now offered at a number of our laboratories. Core photos are provided on discs but are also available for viewing with our on-line Core Photo Album in Webtrieve.
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Accurate results begin with representative samples. Meticulous care is taken in the collection of geological or other samples to provide representative samples to the laboratory. Following sample collection, appropriate laboratory sample preparation protocols must be selected with care to produce the desired homogeneous subsample for analysis. ALS Minerals approaches sample preparation with the same rigorous quality control procedures and careful attention to detail as any other stage of analysis.
The preparation process is designed to produce a small, representative and homogeneous sub-sample from the material you submit to the laboratory. Sample preparation schemes are available to suit most purposes but can also be readily customised to suit any particular project requirement. ALS Minerals staff are accustomed to adapting to specialised procedures and are very aware of the significance that variations in certain steps can have on analytical outcomes. In particular, it is helpful to advise us of mineralised samples that require special handling or special equipment cleaning cycles to eliminate contamination of other samples that might follow in a batch.
SAmPLE PREPARATION
4
APPlicATion
All sample types.
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PKP-21
Price ($)
By quotation
Sample Submission
Please send your samples to any of the addresses on our website and those listed on the back cover page of this document. Preaddressed adhesive labels and sample submission forms are available on our website and can be sent to you on request as well. We can also offer advice on shipping your samples to any of our laboratories by surface carrier, air cargo and air express. Detailed information on requirements and regulations for each jurisdiction are on the website.
Sample Tracking
ALS Minerals is very aware of the value of your samples. Confidence and security in the chain of custody for your samples as they pass through our system is obviously very important. To provide complete traceability your samples are logged into our proprietary world-wide laboratory information management system and given a barcode at log-in. A per sample fee is applicable and is included in the Sample Preparation Packages quoted on the following page. We encourage clients to barcode samples prior to sending them to our laboratories. In such cases we will work with your barcodes. Alternatively, we can attach an ALS Minerals system barcode as your samples are received.
DeScriPTion
Log sample in tracking system and weigh. Samples received with barcode labels attached to sample bag. Samples received without barcode labels attached. Workorder /administration fee applied per submittal. Waste disposal levy One-time charge for each group of samples submitted All Samples. All Samples. LOG-21 LOG-22 BAT-01 LEV-01 no charge 0.60 31.50 0.75
APPlicATion
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APPlicATion
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PREP-31 PREP-31b PREP-32
SAmPLE PREPARATION
APPlicATion
For rock or drill samples with a nominal particle size of <10 mm. (Samples that are coarser will require crushing prior to processing. See page 6 for available options).
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PUL-22 PUL-23 PUL-24
* Splitting charges will only apply to samples >3kg. ** Bagging charges only apply to samples >3kg where both fine pulverised bulk residue and crushed residue are to be retained. ***PUL-23 is the default sample preparation method and will apply in all cases where specific codes are not requested for samples exceeding 1kg in weight.
APPlicATion
Soil or sediment samples.
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PREP-41
Sample Storage
Materials submitted for analysis are retained free of charge at our laboratories for a limited time. Prepared master pulps are stored for 90 days from the time we issue the final Certificate of Analysis. Coarse and fine reject (residue) fractions are stored for 45 days from the time we issue the final Certificate of Analysis. Reasonable monthly charges will apply to samples stored for longer periods in our facilities. ALS Minerals storage facilities provide a secure and organised environment protected from the elements and the sun. ALS Minerals also provides climate controlled storage environments where required, including freezer storage for unstable samples. All sample storage locations are included in the laboratory tracking system so that all your samples for all your projects can be located to the rack and shelf location in any of our facilities world-wide at all times.
DeScriPTion
Monthly storage of bulk residues (<3kg of coarse reject or finely pulverised material) after the first 45 days. Monthly storage of master pulps after the first 90 days. Monthly storage of screening reject fractions after the first 45 days. Handling and retrieval of stored samples. Disposal of pulps and coarse fractions. Return of samples to client.
APPlicATion
Storage of remaining sample after the first 45 days from the issue date of the final certificate of analysis. Longer term storage of pulps. Longer term storage of screening reject fractions. Stored samples. Pulps and coarse fractions. Returned samples.
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STO-REJ STO-PUL STO-SCR RET-21 DIS-21 RTN-21
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Drying
Drying charges are only applied to samples that are excessively wet. Local laboratory managers will determine the applicability of such charges in consultation with the client, when the samples are received.
DeScriPTion
Drying of excessively wet samples in drying ovens. Drying of excessively wet samples in drying ovens that are controlled to a maximum temperature of 60C Air-drying of samples.
APPlicATion
Default drying procedure for most rock chip and drill samples. Most soil and sediment samples that are analysed for volatile elements. Selective Leach procedures and others.
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DRY-21 DRY-22 DRY-23
Crushing
Jaw crushers may be used where samples are too coarse to be put directly into a large pulverising mill, or where particle size must be reduced prior to splitting.
DeScriPTion
Coarse crushing of rock chip and drill samples to 70% nominal -6mm.
SAmPLE PREPARATION
6
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Used if the material is too coarse for introduction into the pulverising mill and as a preliminary step before fine crushing of larger samples. Standard preparation procedure for samples where a representative split will be pulverised.
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CRU-21 CRU-31
Fine crushing of rock chip and drill samples to 70% -2mm or better.
Splitting
Some samples may require splitting into representative subsamples. In many locations automated rotary splitters can be attached to crushers to produce demonstrably superior precision in sub-sample analyses. The addition of rotary splitting eliminates one of the largest systemic sources of error in the production of a sub-sample for analysis.
DeScriPTion
Split sample using a riffle splitter. Split sample using a rotary splitter.
APPlicATion
Standard splitting procedure. Premium splitting procedure.
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SPL-21 SPL-22
Pulverising
All pulverising procedures make use of flying disk or ring and puck style grinding mills unless otherwise specified. Grinding procedures guarantee that, for most sample types, at least 85 percent of the sample material will be pulverised to 75 micron (200 mesh) or better.
DeScriPTion
Pulverise a split or total sample of up to 250g to 85% passing 75 micron or better. Pulverise a 1,000g split to 85% passing 75 micron or better. Pulverise the entire sample to 85% passing 75 micron or better.
APPlicATion
Default procedure for samples that are finely crushed and split prior to pulverising or for total samples up to 250g. Pulverising of a 1kg split or total sample up to 1kg. Appropriate for samples up to 3kg.
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PUL-31 PUL-32 PUL-21
Pulverising bowls are made from a low chrome steel. Other bowls are also available for non-metallic sample preparation (i.e. tungsten carbide, agate , zirconia etc.). Please enquire if interested in non-metallic pulverisation media.
Screening
Screening is performed where a sample needs to be separated into size fractions. Mesh sizes can be specified and custom multiplescreening procedures are available.
DeScriPTion
Sieve sample to -180 micron(80 mesh). Retain both fractions.
APPlicATion
Soil or sediment samples.
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SCR-41+
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SAmPLE PREPARATION
DeScriPTion
Specific Gravity on solid objects Specific Gravity on solid objects after wax coating Specific Gravity on pulps Bulk Density Bulk Density after wax coating
ranGe
0.01 20g/cm3 0.01 20g/cm3
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OA-GRA08 OA-GRA08a OA-GRA08b OA-GRA09 OA-GRA09a
Miscellaneous Procedures
DeScriPTion
Compositing of two or more pulp samples, including homogenising the composite pulp. Volumetric procedure. Compositing of two or more pulp samples, including homogenising the composite pulp. Gravimetric procedure. Clean crushers with barren material after every sample.
APPlicATion
The volumetric is the standard procedure. The gravimetric is used when the densities of the samples vary greatly. As required. (The standard procedure uses compressed air cleaning between samples and barren material between each batch). As required. (The standard procedure uses compressed air cleaning between samples and barren material between each batch). Tray drying of samples submitted in plastic bags. For samples submitted in plastic bags or damaged bags. Re-homogenisation of samples including samples from long term storage.
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CMP-21 CMP-22 WSH-21
Transfer sample to drying tray or new sample bag, applicable to samples requiring tray drying. Re-bagging sample in new bag. Homogenise stored or composite sample by light pulverising.
Quarantine (heat treatment, storage). Required for relevant samples AQIS approved heat treatment and storage. imported into Australia.
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Gold and other precious metals continue to be highly sought after by mining and exploration companies worldwide as a result of their strong prices in recent years. ALS Minerals has the analytical tools and years of experience to help you with this potentially valuable search.
Selection of the best method for the accurate determination of precious metal content in a sample is highly dependent on the nature of the sample matrix, the grain size and distribution of the precious metals of interest and the objective of the analytical result.
Gold
Fire Assay Fusion
For quantitative analysis of gold, the fire assay procedure is still the preferred choice globally. However, it should also be recognised that a wide variety of minerals and metals such as chromite, base metal sulfides and oxides, selenides and tellurides in moderate to high concentrations, can interfere with the fire assay process, generally leading to low precious metal recoveries. With prior knowledge of the presence of these minerals and metals, ALS Minerals can modify flux constituents and increase flux to sample ratios to improve recoveries. In most cases, a reduction in sample weight will yield higher precious metal recoveries, particularly in the presence of the interfering species mentioned above. For optimum gold and PGE recoveries for most sample matrices, ALS Minerals recommends a 30g maximum charge weight.
AnAlyTe
Au
ranGe (ppm)**
0.001-10
DeScriPTion
Au by fire assay and ICP-AES. 30g nominal sample weight 50g nominal sample weight Au by fire assay and AAS. 30g nominal sample weight 50g nominal sample weight Au by fire assay and AAS. 30g nominal sample weight 50g nominal sample weight Au by fire assay and AAS. 30g nominal sample weight 50g nominal sample weight Au by fire assay and gravimetric finish. 30g nominal sample weight 50g nominal sample weight Au and Ag by fire assay and gravimetric finish. 30g nominal sample weight 50g nominal sample weight 1 kg.screen fire assay. Screen to 100 micron. Duplicate assay on screen undersize. Assay of entire oversize fraction. 30g nominal sample weight 50g nominal sample weight
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trace Level
Au-ICP21 Au-ICP22 Au-AA21 Au-AA22 Au-AA23 Au-AA24 14.20 15.25 14.20 15.25 12.60 13.15
Au
0.002-1
Au
0.005-10
Ore Grade
Au 0.01-100 Au-AA25 Au-AA26 Au-GRA21 Au-GRA22 ME-GRA21 ME-GRA22 11.55 12.10 23.10 25.20 28.90 31.50
Au
0.05-1,000
Au Ag Au
Au-SCR21* Au-SCR24*
90.30 102.95
* Other screen sizes may be available - please contact your local office for details. ** 1 oz/ton = 34.2857 ppm
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AnAlyTe
Au
ranGe (ppm)*
0.07-999,985
DeScriPTion
Au by fire assay and gravimetric finish. 30g nominal sample weight Routine bullion assays by fire assay with gravimetric finish. Au umpire assay in bullion samples by fire assay with gravimetric finish.
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Concentrates
Au-CON01 POA
Bullion
Au Au Fineness 0.1-1,000 Fineness 1-1,000 Au-GRA24 Au-UMP20 200.00 395.00
*At your request, precious metals reporting units can be specified as ppb, ppm, g/t or oz/t (except for bullion assays).
ranGe (ppm)
0.0001-0.1
DeScriPTion
Au by aqua regia, ICP-MS (MARG). 25g nominal sample weight 50g nominal sample weight Au by aqua regia extraction with ICP-MS finish. 25g nominal sample weight 50g nominal sample weight 15g nominal sample weight Au by aqua regia extraction with AAS or ICP-MS finish. 25g nominal sample weight 50g nominal sample weight Samples containing sulfidic, calcareous or organic material
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trace Level
Au 0.001-1 Au-TL43 Au-TL44 Au-TL42 12.10 13.15 11.00
Ore Grade
Au 0.01-100 Au-OG43 Au-OG44 RST-21 8.65 9.70 2.90
Roasting
Au
* Additional acid leachable elements by ICP-AES can be added at a competitive price. See pages 13 and 14 for details.
ranGe (ppm)
0.0001-0.1
DeScriPTion
Au by Aqua Regia with ICP-MS finish + MS-MS41 25g nominal weight 50g nominal weight Au by Aqua Regia with ICP-MS finish + ME-MS41 15g nominal weight 25g nominal weight 50g nominal weight
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ST43-PKG ST44-PKG TL42-PKG TL43-PKG TL44-PKG
0.001-1
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Cyanide Leach
Cyanide leach procedures are used in grassroots exploration where cyanide extraction from a very large sample can sometimes detect small gold anomalies that otherwise would go unnoticed. In mine development and exploration, this procedure can be used to establish the potential gold cyanide extraction efficiency.
AnAlyTe
Au Au
ranGe (ppm)
0.0001-10 0.0001-10
DeScriPTion
BLEG Au-cyanide leach with ICP-MS finish. 1,000g nominal sample weight BLEG Au-cyanide leach with extraction AA finish. 1,000g nominal sample weight BLEG Au-cyanide leach with ICP-MS finish. 500g nominal sample weight BLEG Au-cyanide leach with extraction AA finish. 500g nominal sample weight Au by cyanide leach with AAS finish. 30g nominal sample weight Au by cyanide leach with AAS finish. 1,000g nominal sample weight Au by accelerated cyanide leach using LeachWELL reagent with AAS finish. 500-3,000g nominal sample weight
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trace Level
Au Au 0.001-10 0.001-10 Au-CN11* Au-AA11* 25.40 25.40
Ore Grade
Au Au Au 0.03-50 0.01-200 0.01-300 Au-AA13* Au-AA14* Au-AA15 15.60 25.40 32.90
*The following additional elements can be reported on request at additional cost. Ag (0.001), Cu (0.01), Pd (0.001) on method Au-CN12 Ag (0.001), Cu (0.01), Pd (0.001) on method Au-CN11 Ag (0.03), Cu (0.1) on method Au-AA13 1.75/element 1.75/element 1.75/element
Metallurgical Samples
AnAlyTe
Au
ranGe (ppm)
0.01-50
DeScriPTion
Au in cyanide liquor by extraction with AA finish.
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Au-AA16
Note: A full range of minor and trace elements can be determined on cyanide liquors by ICP-AES/ICP-MS. Please enquire for details. Au 1-10,000 Au on carbon by ashing, aqua regia digestion and AAS. Duplicate analysis. Au-AA44 43.90
Note: A range of elements can be determined on the ashed carbon by ICP-AES/ICP-MS. Please enquire for full details.
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Silver
AnAlyTe ranGe (ppm)
0.2-100 0.5-100
DeScriPTion
Ag by aqua regia digestion and AAS. Ag by HF-HNO3-HClO4 digestion, HCl leach and AAS.
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Ag-AA45 Ag-AA61
trace Level
Ag Ag
Note: See also multi-element methods that include Ag under Exploration Geochemistry (pages 12-15).
Ore Grade
Ag Ag Ag 1-1,500 1-1,500 5-10,000 Ag by aqua regia digestion, ICP-AES or AAS finish. Ag by HF-HNO3-HClO4 digestion with HCl leach, ICP-AES or AAS finish. Ag by fire assay and gravimetric finish. 30g nominal sample weight 50g nominal sample weight Au and Ag by fire assay and gravimetric finish. 30g nominal sample weight 50g nominal sample weight Ag by fire assay and gravimetric finish. Routine bullion assays by fire assay with gravimetric finish. Ag umpire assay in bullion samples by fire assay with gravimetric finish. Ag-OG46* (Ag-AA46) Ag-OG62* (Ag-AA62) Ag-GRA21 Ag-GRA22 ME-GRA21 ME-GRA22 Ag-CON01 11.55 15.35 25.00 30.00
Au Ag
0.05-1,000 5-10,000
Concentrates
Ag 0.7-995,000 Fineness 1-1,000 Fineness 1-1,000
Bullion
Ag Ag Ag-GRA24 Ag-UMP20 200.00 395.00
DeScriPTion
Pt, Pd and Au by fire assay and ICP-AES finish. 30g nominal sample weight 50g nominal sample weight Pt, Pd and Au by fire assay and ICP-MS finish. 30g nominal sample weight 50g nominal sample weight Pt, Pd, Ir, Os, Rh, Ru and Au by fire assay with nickel sulfide collection and neutron activation analysis. 30g nominal sample weight Note: Au is not quantitative by this method. Pt, Pd and Au by fire assay and ICP-AES (or ICP-MS) finish. 30g nominal sample weight
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trace Level
Pt Pd Au Pt Pd Au Pt Pd Ir Os Rh Ru Au PGM-ICP23 PGM-ICP24 PGM-MS23 PGM-MS24 19.05 21.35 23.10 25.40
PGM-NAA26
POA
Ore Grade
Pt Pd Au PGM-ICP27 21.35
At your request, precious metals units can be reported as ppb, ppm, g/t or oz/t (except for bullion assays). To achieve optimum PGE recovery for most sample matrices, ALS Minerals recommends a 30g charge weight.
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Exploration geochemistry utilises trends and patterns in trace elements as indicators of what may lie deep below the surface or at great distance from the current location. More and more often, todays explorers require lower detection limits and a wider range of elements to identify prospective targets.
The effectiveness of a geochemical exploration program is largely dependent on the availability of analytical methods that properly meet the requirements of the problems at hand. Element coverage, detection limits, reliability and cost are often the main factors considered by explorers when choosing an analytical method for a given sample type. ALS Minerals offers a wide range of multi-element and single-element methods that can satisfy the requirements of todays exploration geochemists, both technically and economically. The analytical methods described in this section include different sample decomposition procedures, such as aqua regia and multi-acid digestions, fusions and selective leaches. The instrumental analytical techniques include inductively coupled plasma with atomic emission spectroscopy or mass spectroscopy, atomic absorption, x-ray fluorescence and infrared spectroscopy.
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Note: To include Hg by a separate procedure in the suite of elements above, please request ME-MS61m instead of ME-MS61.
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Note: To include Hg to a lower detection limit of 0.01ppm in the suite of elements above, please request method ME-ICP41m instead of ME-ICP41.
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Note: To include Hg in the suite of elements above, please request method ME-ICP61m instead of ME-ICP61.
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50-50,000 50-50,000 5-50,000 50-50,000 10-50,000 ME-ICP41a 24.15 complete package or 11.25 plus 2.50/element
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The procedures listed below are designed to provide optimum results for each While analytical methods for geochemical exploration are optimised for low ore type or product. assays for evaluation of ores and high grade materials are detection limits, the This includes the specific digestion procedure, calibration protocols and accuracy and precision atCertified Reference Materials for each optimised for the use of appropriate high concentrations. sample type. For large projects or regular submissions of certain products, where a broader element suite or lower detection limits are required, ALS will consider of Ores & High Grade Materials evaluation customising methods to suit individual needs.
The methods described in this section are suitable for most ores and high grade materials. Depending on the purpose of the analytical results, concentrations greater than 15%-20% may require the use of more expensive methods, such as titrimetric and gravimetric analysis, in order to achieve the maximum accuracy. Please contact your nearest ALS laboratory should you require this type of analysis. For characterisation of ores, recommended procedures include; the aqua regia digestion (OG46) primarily for lead/silver/zinc rich ores and four acid digestion method (OG62) for copper and zinc ores with low lead and silver and nickel laterite ores. Samples expected to contain significant amounts of sulfides of copper, nickel and/or cobalt are fused with sodium peroxide and then leached with dilute hydrochloric acid using procedure ICP81. High grades of elements difficult to solubilise or maintain in solution, such as barium, tungsten, are best done by XRF. The mineralogy of the sample as well the elements to be determined should be considered when selecting an assay procedure.
Acid Digestions
Aqua regia digestion is a powerful solvent for sulfides, which dissolves Ag and the base metals but the resistive mineral forms are not completely dissolved. Aqua regia digestion with iCP-AeS or AAS Finish
anaLyTeS & ranGeS (%)
Ag As Cd 1-1,500ppm 0.01-60 0.0005-10 Co Cu Fe 0.001-20 0.001-40 0.01-100 Mn Mo Ni 0.01-50 0.001-10 0.001-10 Pb S Zn 0.001-20 0.01-10 0.001-30
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(+)-OG46 (+)-AA46
Four Acid Digestion, using HF, is a very strong digestion method which almost completely breaks down silicates which are volatised as SiF4. The digestion will decompose all but the most resistive minerals. Four Acid digestion with iCP-AeS or AAS Finish
anaLyTeS & ranGeS (%)
Ag As Bi Cd 1-1,500ppm 0.001-30 0.001-30 0.0005-10 Co Cr Cu Fe 0.001-20 0.002-30 0.001-40 0.01-100 Mg Mn Mo Ni 0.01-50 0.01-50 0.001-10 0.001-30 Pb S Zn 0.001-20 0.01-10 0.001-30 (+)-OG62 (+)-AA62 12.20 plus 3.15/element 12.20 plus 3.15/element
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Fusions
Sodium peroxide fusions are effective for the decomposition of sulfides, arsenides and many refractory minerals such as chromite, rutile, ilmenite and titanite. It is the method of choice for nickel sulfide deposits. Sodium Peroxide Fusion with iCP-AeS Finish
anaLyTeS & ranGeS (%)
Al As Ca Co 0.01-50 0.01-10 0.05-50 0.002-30 Cr Cu Fe K 0.01-30 0.005-30 0.05-100 0.1-30 Mg Mn Ni Pb 0.01-30 0.01-50 0.005-30 0.01-30 S Si Ti Zn 0.01-60 0.1-50 0.01-30 0.01-30 (+)-ICP81 35.00 complete package or 20.00 plus 3.15/element
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XRF analysis is the preferred method for highly resistive elements. A homogenous glass disc is prepared by fusion, eliminating mineralogical effects. It has particular applications for resistive minerals and the determination of elements that are difficult to decompose and retain in stable solutions at high concentrations Lithium Borate Fusion with XrF Finish
anaLyTeS & ranGeS (%)
Ba Nb Sb 0.01-50 0.01-10 0.01-50 Sn Ta Th 0.01-60 0.01-50 0.01-15 U W Zr 0.01-15 0.01-50 0.01-50 (+)-XRF10 25.00 plus 3.15/element
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Iron Ore represents a large proportion of the worlds bulk mining and exploration activity. In its metal form, iron constitutes 95% of all metals used by modern industrialised society. Common mineral forms which are amenable to bulk mining include hematite, magnetite, goethite/limonite, siderite, chamosite, pyrite and ilmenite. The oxide mineral forms contribute the largest percentage of iron ore to global production.
DeScriPTion
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Loss on Ignition LOI (0.01%) at 371C, 425C, 550C, 650C and 1000C Moisture @ 110 C
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DTR Fe-VOL05 MAGSP-01
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COnCenTrATeS MinerALOGy
OTher ServiCeS
Aluminium is the most abundant metal element in the earths crust. Bauxite is the most common ore from which alumina is commercially extracted. Gibbsite, boehmite and diaspore are the predominant aluminium rich minerals which co-exist with goethite, hematite and kaolinite in bauxite ore.
DeScriPTion
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DeScriPTion
TOC by LECO. Microwave digestion, chemical separation/ICP-AES analysis.*
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C-IR17 Si-LICP01 Al-LICP01
*Digestion temperature, caustic strength and sample weight/caustic strength ratio to be specified by client.
DeScriPTion
Client specific procedure. Wet screening using 600mm diameter Kason Screen
coDe
n/a Various depending on screen size requested
Multiple Screen Analysis Screens available: 300m 1200m 2500m 600m 1700m 7000m 900m 1900m 9600m Moisture Content (%) Pulverise sub-sample
SCR-34
12.60* /screen
OA-GRA05g PUL-32
5.25 6.05
*Additional costs apply to recovery of fines from beneficiated sample. Percentage recovery reported under relevant screen code.
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Evaluation of copper prospects may involve the need to know more about copper mineralogy and mineral solubility for metallurgical considerations. The separation of oxide/carbonate, secondary chalcocite and primary sulfide minerals compared to the total copper are useful in determining leachability of copper in a deposit. This information can be obtained by sequential leaching of the sample and may be augmented by direct mineralogical determination using MLA applied mineralogy.
copper Procedures
Copper oxide minerals such as malachite, azurite, chrysocolla and portions of cuprite and tenorite can be leached using sulfuric acid, referred to as acid soluble copper. Cyanide leach will dissolve the secondary chalcocite, bornite and a portion of the chalcopyrite content of the sample, while the majority of the sulfide minerals will remain in the residue analysed at the end of a sequential leach. The mineral dissolution in each leach may vary depending on the sample matrix and specific mineralogy. ALS Minerals provides custom methods using different leach conditions upon request.
AnAlyTe coDe
Cu-AA45 Cu-AA61 Cu-AA46 Cu-OG46 Cu-AA62 Cu-OG62 Cu-CON02 Cu-VOL61 Cu-AA04 Cu-AA05 Cu-AA07n Cu-AA08n Cu-AA17a Cu-PKG06LI
Trace Cu Methods
Trace Cu method, aqua regia digestion and ICP or AAS finish, 1-10,000 ppm. Trace Cu method, 4 acid near total digestion and ICP or AAS finish, 1-10,000 ppm.
Assay Cu Methods
Assay Cu method, aqua regia digestion and ICP finish, 0.01-40%. Assay Cu method, 4 acid near-total digestion and ICP finish, 0.01-40%. 11.55 15.35
Concentrate Cu Method
HNO3-HCl-H2SO4 acid digestion followed by potentiometric titration, done in duplicate, 0.01-100%. HNO3-HCl-HF-H2SO4 acid digestion followed by volumetric finish, done in duplicate, 0.01 to100% 84.00 63.00 11.35 11.35 11.35 11.35 13.60 42.00
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OTher ServiCeS
ALS Minerals has developed a variety of analytical methods suitable for the analysis of nickel in laterite and sulfides. These methods have been tailored to suit the mineralisation style and the specific sample type, whether exploration, resource definition or mine grade control.
nickel Procedures
Acid Digestion techniques
First pass exploration samples are often analysed using method ME-ICP61 which is a four acid digestion technique with ICPAES finish. While the method has an upper detection limit of 1% for nickel, it is recommended that an ore grade method (ie method Ni-OG62) is used to re-assay nickel concentrations exceeding 0.5%, which is a typical lower cut-off grade.
anaLyTeS & ranGeS (%) coDe
Ni-ICP61
Trace ni Method
Ni Ni Al As 1-10,000ppm 0.01-30 0.01-50 0.01-30 Ni by HF-HNO3-HClO4 digestion, HCl leach and ICP-AES/AAS. Bi Ca Co 0.01-30 0.01-50 0.001-20 Cr Cu Fe 0.002-30 0.001-40 0.01-100 Mg Mn S 0.01-50 0.01-50 0.01-50 ME-OG62 12.20 plus 3.15/element
Assay ni Method
* Additional elements are available on these methods. Refer to Exploration & Ore Grade pages.
Fusion techniques
The industry preferred technique for resource definition of lateritic ore deposits is X-Ray Fluorescence (XRF). A finely pulverised sample is fused with lithium borate to produce a uniformly sized glass disc suitable for presentation to the XRF Spectrometer. The comprehensive analysis of laterite ores for major and minor elements is critical in evaluating project economics and for metallurgical process control. Loss On Ignition (LOI) determination using a Thermo Gravimetric Analyser (TGA) is also an important component of the total analysis. For nickel sulfide ores, a sodium peroxide fusion technique with ICPAES finish (method ME-ICP81) is recommended to replace the borate fusions typically used for lateritic ores. Fusion XrF for Laterite Ore
anaLyTeS & ranGeS (%)
Al2O3 CaO Co Cr2O3 Cu 0.01-100 0.01-40 0.001-7 0.005-10 0.001-1.6 Fe2O3 K 2O MgO MnO Na2O 0.01-100 0.01-6.3 0.01-50 0.005-30 0.01-5.3 Ni P 2O 5 Pb SiO2 TiO2 0.005-7.8 0.005-23 0.005-1.8 0.05-100 0.01-30 LOI 1000C Zn 0.001-1.6
DeScriPTion
Fused disc XRF and TGA for Loss on Ignition
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ME-XRF12n (normalised) ME-XRF12u (unnormalised)
DeScriPTion
Sodium Peroxide fusion/ICPAES finish
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ME-ICP81
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OTher ServiCeS
In addition to an understanding of deposit occurrence, uranium exploration now also requires an awareness of the issues and hazards that might be associated with Naturally Occurring Radioactive Materials (NORM) so that these materials are dealt with in a responsible manner.
Uranium Procedures
ALS has standardised screening and handling protocols throughout its network of laboratories to ensure that any NORM samples received can be rapidly identified and are handled in a manner meeting all appropriate regulations with respect to transportation, workplace safety and environmental regulations. uranium in non-resistate Minerals & Soils by Aqua regia digestion
anaLyTe & ranGeS
51 elements including U (0.05 - 10,000 ppm). Elements and ranges are summarised in the table for method ME-MS41 on page 13.
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ME-MS41u
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ME-MS61u
ranGe (ppm)
4-10,000 0.01%-15% 0.2-10,000
DeScriPTion
U by pressed pellet, XRF. U by lithium borate fusion, XRF. U by neutron activation.
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U-XRF05 U-XRF10 U-NAA05
Use of lithium has migrated from the classical use in glass and ceramics to batteries for portable electronics and cars. This has led to a renewed interest in lithium as a target for exploration.
Lithium Procedures
Lithium may occur with salt, carbonates, phosphates or sulfates in brines and clay sequences in evaporate deposits. It occurs within the mica pelidolite and within spodumene and clays such as hectorite, most easily substituting in many minerals for Mg. Pathfinder elements of interest may include K, Mg, B, F, Na and Ca. Lithium Mineral Analysis
anaLyTe & ranGeS
Four acid sample digestion with determination by ICP-AES and ICP-MS for 48 elements (see page 13). Li range of 0.2 - 10,000 ppm. Li by four acid digestion/ICP-AES analysis, Li range 10-10,000 ppm. Assay method for Li by specialised 4-acid digestion, range 0.01-10% Li.
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ME-MS61 Li-ICP61 Li-OG63
Brine Analysis
anaLyTe & ranGeS
Lithium Brine Analysis by ICP-AES. 27 elements including Li (50 mg/L to 3000 mg/L). Trace Brine Analysis by ICP-MS, 36 elements, Li range 10 ug/L to 500 mg/L. Brine determination of for pH, conductivity, total dissolved solids, total alkalinity.
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ME-ICP15 ME-MS14b Li-BrPKG
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OTher ServiCeS
The storage of overburden, waste rock and mine waste materials at mine sites must be carefully planned to minimise the environmental impact of mining operations. Samples may be tested to predict their acid producing or neutralising potential, thus allowing responsible mine planning.
SOBek MeTHOD PaCkaGe CODe aBa-PkG01 (M/S) aBa-PkG02 (M/S) aBa-PkG03 aBa-PkG04 aBa-PkG05
**The standard package uses the Sobek, EPA Neutralisation Potential Method Add the (M) to the package for the Modified Neutralisation Potential Method of Lawrence Add a (S) to the package name for the Siderite Correction of Skousen
Mineralogy of the sample will affect the accuracy of the ABA prediction. The presence of siderite (iron carbonate) may overestimate neutralising potential of a sample if acid is introduced. Sulfates such as gypsum and barite will cause overestimation of the sulfur if a total sulfur measurement is used. Some samples may contain minerals which are not sulfide but which are acid-producing. There are carbonate minerals that do not neutralise the sample, as well as non-carbonate buffering minerals such as biotite and chlorite. Mineralogical knowledge of the sample is an important augmentation to the static ABA tests.
DeScriPTion
Net Acid Generation (NAG) - Hydrogen peroxide is used to facilitate the rapid oxidation of sulfide. NAG is reported in kg H2SO4/tonne at pH 4.5 and pH 7.0.
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OA-VOL11
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OTher ServiCeS
Exploration for deposits of rare earth elements (REEs) is booming. Due to the REEs unique ability to retain their physical properties at high temperatures, they are critical components of materials used in electronics, hybrid batteries, wind turbines and other key industries. Demand for these products will only increase the demand for REEs.
Exploration now requires methods that cover a range of concentrations from the lowest detectable levels up to percentage level concentrations.
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Combination of Rare Earth & Trace Elements from method ME-MS81 plus whole rock package by method ME-ICP06.
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(+)-OGREE
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Analysis related to lithogeochemistry, alteration minerals and trace element mobility are important tools in understanding geological environments. The selections of analytical packages on this page are designed to offer comprehensive information for these studies.
The nature of lithophile elements and the matrices in which they occur require stronger dissolution procedures to separate them from the bulk matter. The most accurate results will therefore be obtained using fusion as the separation procedure or through direct analysis. X-ray fluorescence (XRF) is the preferred technique; however, ICP-AES can also be effectively used following a fusion.
DeScriPTion
Lithium metaborate fusion, ICP-AES By Leco Four Acid, ICP-AES Lithium borate fusion, ICP-MS Aqua regia, ICP-MS
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CCP-PKG01
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Aqua regia digestion is a cost effective method for determining the acid leachable portion of elements. Sample minimum size is 1 g.
anaLyTeS & ranGeS (ppm) coDe Price Per SAmPle ($)
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ranGe (ppm)
0.01%-50% 0.02%-50% 0.02%-50% 0.01%-50% 0.01%-50% 0.01%-50% 0.01%-50% 0.01%-50%
DeScriPTion
Total carbon by Leco furnace. Dilute acid digestion followed by Leco furnace. Carbonate carbon by difference. Total Carbon and total Sulfur by Leco furnace. Total sulfur by Leco furnace. Sulfate Sulfur by dilute Hydrochloric acid digestion and ICP-AES analysis. Sulfide Sulfur calculated by difference between total and sulfate sulfur.
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C-IR07 C-IR17 C-CAL15 ME-IR08 S-IR08 S-ICP16 S-CAL07
halides
AnAlyTe
Br** Cl Cl Cl F F I**
ranGe (ppm)
0.5-10,000 100-10,000 10-40,000 0.01-80% 20-20,000 0.01%-100% 0.5-10,000
DeScriPTion
Neutron activation. Neutron activation. Fusion - XRF. Acid Digestion titrimetric finish Fusion - S.I.E. Fusion - S.I.E. Neutron activation.
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Br-NAA05 Cl-NAA06 Cl-XRF11 Cl-VOL66 F-ELE81a F-ELE82 I-NAA07
Other
AnAlyTe
FeO Hg pH Conductivity H2O- (Moisture) H2O+ (Water of Crystallisation) LOI
ranGe (ppm)
0.01%-100% 0.01-100 1-100,000 s/cm 0.01%-100% 0.01%-100% 0.01%-100%
DeScriPTion
Ferrous iron by H2SO4-HF acid digestion and titrimetric finish. Aqua regia digestion, ICP-MS. Soil pH (1:1 ratio). 5g minimum. Conductivity of soil extract. 5g minimum. Gravimetric procedure after drying at 105C. By Leco. LOI at 1000C.
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Fe-VOL05 Hg-MS42 OA-ELE05 OA-ELE04 OA-GRA10 OA-IR06 OA-GRA05
* Sulfur may be understated if BaSO4 or SrSO4 present. ** A surcharge may apply for batches of less than 20 samples.
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Ionic Leach
This sodium cyanide leach is buffered to pH 8.5 using the chelating agents ammonium chloride, citric acid and EDTA. Ionic Leach enables the detection of buried mineralisation using a surface regolith or soil, through the dissolution and subsequent measurement of weakly bound ions loosely attached to surface particles. The ability of this innovative leach to give close to true background detection limits makes it effective in providing geochemical contrast and targeting buried mineralisation. The method requires 50 grams of sample. Selective, ph controlled leach with iCP-MS analysis and final ph measurement
AnAlyTeS (ppm)
Ag As Au Ba Be Bi Br Ca Cd Ce Co Cr Cs Pb 206 0.0001 0.002 0.00002 0.01 0.0002 0.003 0.05 0.2 0.001 0.0001 0.0003 0.001 0.0001 0.001 Cu Dy Er Eu Fe Ga Gd Ge Hf Hg Ho I In Pb 207 0.001 0.0001 0.0001 0.0001 0.1 0.0005 0.0001 0.0001 0.0005 0.0001 0.0001 0.01 0.0001 0.001 La Li Lu Mg Mn Mo Nb Nd Ni Pb Pd Pr Pt Pb208 0.0001 0.0002 0.0001 0.01 0.01 0.0005 0.0001 0.0001 0.001 0.001 0.0001 0.0001 0.0001 0.001 Rb Re Sb Sc Se Sm Sn Sr Ta Tb Te Th Ti 0.0001 0.0001 0.0005 0.001 0.002 0.0001 0.0002 0.001 0.001 0.0001 0.001 0.00002 0.005 ME-MS22 30.00 plus 1.40/element Tl Tm U W Y Yb Zn Zr 0.0005 0.0001 0.0001 0.001 0.0001 0.0001 0.01 0.0001 pH controlled ionic leach with analysis by ICP-MS including final pH ME-MS23 50.00 Complete package
DeScriPTion
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Ammonium Acetate
A buffered ammonium acetate leach is used to extract exchangeable ions and carbonates. Slightly stronger than a water wash, this very weak leach targets the most weakly bound ions and may be used in sequential extractions prior to stronger leaches.
Sodium Pyrophosphate
Organic matter in soils and sediments is capable of forming chelation complexes with metals. A solution of neutral (pH 7) sodium pyrophosphate liberates these organically-bound heavy metals. Variations in the concentrations of organically-bound metals such as copper, zinc, cobalt, nickel, iron and aluminium have been used as indications of buried mineral deposits. Extraction with pyrophosphate does not attack sulfides, nor does it dissolve significant amounts of amorphous iron oxides
anaLyTe & LOwer rePOrTInG LIMITS (ppm)
Ag Al As Au B Ba Be Bi Br Ca Cd Ce Co Cr Cs Cu Dy Er Eu Fe Ga 0.002 1 0.1 0.05 2 0.05 0.05 0.005 2 10 0.01 0.005 0.05 0.05 0.005 0.05 0.005 0.005 0.005 5 0.05 Gd Ge Hf Hg Ho I In K La Li Lu Mg Mn Mo Na Nb Nd Ni P Pb Pr 0.005 0.1 0.01 0.1 0.005 0.1 0.005 5 0.005 0.05 0.005 1 0.1 0.01 10 0.01 0.005 0.05 5 0.1 0.005 Rb Re Sb Se Sm Sn Sr Ta Tb Te Th Ti Tl Tm U V W Y Yb Zn Zr 0.01 0.001 0.005 0.5 0.005 0.05 0.05 0.01 0.005 0.05 0.01 1 0.005 0.005 0.005 0.05 0.01 0.005 0.005 0.2 0.05 Sodium pyrophosphate leach with ICP-MS. ME-MS07 47.25 Hot hydroxylamine hydrochloride leach with ICP-MS. ME-MS06 47.25 Cold hydroxylamine hydrochloride leach with ICP-MS. ME-MS05 47.25 Ammonium acetate. ME-MS04 47.25
DeScriPTion
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Sample media such as vegetation and waters have been shown to provide valuable information for exploration programs. Trace element levels in these sample types are often at extremely low levels. Effective analytical procedures require the utmost care in sample preparation and analysis to ensure suitable data quality.
Biogeochemistry Procedures
Results are reported on vegetation samples following a nitric/hydrochloric acid digestion on 1g of sample. Custom designed tubes are used to provide maximum reflux of acids. Certified reference materials are included in the analysis of each group to validate accuracy. ALS offers customised preparation of vegetation samples out-sourced to a specialty laboratory. Preparation price varies according to type of sample. Due to permit requirements, vegetation samples will be held for 45 days and are not available for return to the client.
anaLyTeS & ranGeS (ppm)
Ag Al As Au B Ba Bi Ca Cd Co 0.002-100 0.01%-25% 0.1-10,000 0.0002-100 10-10,000 0.1-10,000 0.01-10,000 0.01%-40% 0.01-2,000 0.01-10,000 Cr Cu Fe Ga Hg K La Mg Mn Mo 0.1-10,000 0.01-10,000 0.01%-50% 0.05-10,000 0.001-100 0.01%-10% 0.01-10,000 0.001%-30% 1-50,000 0.01-10,000 Na Ni P Pb Pd Pt S Sb Sc Se 0.001%-10% 0.1-10,000 0.001%-5% 0.01-10,000 0.002-100 0.001-100 0.01%-10% 0.02-10,000 0.1-10,000 0.1-1,000 Sr Te Th Ti Tl U V W Zn 0.2-10,000 0.02-500 0.01-10,000 0.001%-10% 0.02-10,000 0.01-10,000 1-10,000 0.05-10,000 0.1-10,000 ME-VEG41 42.00 Sold only as a complete package.
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Hydrogeochemistry Procedures
Geochemical Analysis of Ground Water Samples is available using ICP-MS. Water samples are analysed directly as submitted by inductively coupled plasma-mass spectrometry.
anaLyTeS & ranGeS (ppb)
Ag Al As Ba B Be Bi Ca Cd Ce Co Cr 0.06-1,000 50-10,000 10-1,000 0.01-1,000 10-1,000 0.3-1,000 0.1-1,000 200-10,000 0.1-1,000 0.02-1,000 0.1-1,000 1-1,000 Cs Cu Fe Ga Hf Hg In K La Li Mg Mn 0.01-1,000 0.3-1,000 20-10,000 0.05-1,000 0.05-1,000 0.2-1,000 0.04-1,000 60-10,000 0.02-1,000 10-1,000 4-10,000 0.1-1,000 Mo Na Nb Ni P Pb Rb Sb Se Sn Sr Ta 1-1,000 300-10,000 0.02-1,000 0.5-1,000 100-10,000 0.2-1,000 0.1-1,000 0.1-1,000 10-1,000 0.3-1,000 0.1-1,000 0.01-1,000 Te Th Tl U V W Y Zn Zr 10-1,000 0.01-1,000 0.04-1,000 0.01-1,000 1-1,000 0.2-1,000 0.03-1,000 2-1,000 0.05-1,000 ME-MS14PKG POA Complete package
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Note: Samples with high metal content or brines should be analysed by ME-ICP14.
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OTher ServiCeS
Isotope geochemistry is useful to determine the source and age of geological materials. Improvements in instrument technology now allow the detection limits required to measure a variety of element isotopes, providing a deeper level of understanding of the composition of geological materials. Isotope determinations are increasingly documented to provide unique signatures that relate to specific styles of mineralisation and alteration. Improved technology continues to increase the number of elements for which isotopic abundances may be measured.
isotopes
Isotopic determinations are made using the Sector Field ICP-MS (ICP-SFMS), providing precision of 0.05% relative standard deviation. Even greater precision can be provided by the multi-collector ICP-MS in which simultaneous measurement of the isotopes is made by individual detectors. The MC-ICP-MS can measure precision to 0.001% relative standard deviation.
AnAlyTeS DeScriPTion coDe Price Per SAmPle ($)
Boron Isotopes. Lead Isotopes for origin determinations. Uranium Isotopes. Re/Os dating of sulfide minerals done on molybdenite mineral separates.
Re/Os Dating
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OTher ServiCeS
Analysis of mine concentrate and metallurgical samples is critical for the purchase and sale of commodities as well as the optimisation of the recovery process. With so much riding on a correct result, control assays require meticulous work by highly trained technicians. The results must be of the highest calibre for reliability, accuracy and precision.
ranGe (ppm)*
0.07-999,985 0.7-995,000 Fineness 1-1,000 Fineness 1-1,000
DeScriPTion
Au by fire assay and gravimetric finish. 30g nominal sample weight Ag by fire assay and gravimetric finish. Routine bullion assays by fire assay with gravimetric finish. Au umpire assay in bullion samples by fire assay with gravimetric finish. Routine bullion assays by fire assay with gravimetric finish. Ag umpire assay in bullion samples by fire assay with gravimetric finish.
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Au-CON01 Ag-CON01 Au-GRA24 Au-UMP20 Ag-GRA24 Ag-UMP20
*At your request, precious metals reporting units can be specified as ppb, ppm, g/t or oz/t (except for bullion assays).
ranGe (%)
0.01-100 0.01-100 0.01-100 0.01-100 0.01-100
DeScriPTion
Cu Concentrate - Volumetric. Zn by Titration. Pb by Titration. Total Fe in Concentrates. FeO (Ferrous Iron).
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Cu-VOL61 Zn-VOL50 Pb-VOL70 Fe-VOL51 Fe-VOL05
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Industrial minerals are those whose commercial value does not rely on the production of a metal or fuel from the mineral source. Typical examples include limestone, clay, silica, gypsum and talc. Metallic compounds where used in nonmetallic form such as rutile or titanium dioxide are also included in this group.
industrial minerals
Industrial mineral analysis commonly includes analyses that deal with unusual matrices and highly refractory components. As a result, aggressive digestions are selected to ensure complete homogeneity of the analytical sub-sample leaving no residual sample. We have extensive experience analysing industrial mineral products such as phosphates, beach sands, ilmenites, raw building materials such as limestone and dolomite right through to intermediate processing plant flows and product streams. Typically these analyses are used to characterise the commercial material, identify contaminants and quality variations, and to provide legislative checks for waste acceptance and occupational hygiene purposes. The procedures listed below are designed to provide optimum results for each material type or product. This includes the specific digestion procedure, calibration protocols and the use of appropriate Certified Reference Materials for each sample type. Where a more inclusive element suite or lower detections limits are required, ALS Minerals can customise methods or develop new procedures to suit individual needs.
ore/ProDUcT
Cementitious Materials Glass Sand Products Limestone, Dolomite, Magnesite, Magnesia Manganese Ore Phosphate Rock Silicates Rutile Product
AnAlyTeS
CaO, SiO2, Fe2O3, Al2O3, Mn2O3, Na2O, K 2O, SO3, MgO, TiO2, Cr2O3, P2O5, SrO, LOI SiO2, Fe2O3, Al2O3, Cr2O3, TiO2 CaO, MgO, Al2O3, Fe2O3, SiO2, LOI MnO, Fe2O3, SiO2, Al2O3, P2O5, LOI P2O5, Fe2O3, Al2O3, SiO2, CaO, MgO, TiO2, Na2O, K 2O, MnO, LOI. Al2O3, BaO, CaO, Cr2O3, Fe2O3, K 2O, MgO, MnO, Na2O, P2O5, SiO2, SrO, TiO2, LOI
DeScriPTion
Fusion, ICP-AES Fusion, ICP-AES/ICP-MS Fusion, ICP-AES Fused bead XRF Fused bead, XRF Fused bead, XRF
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ME-XRF12s ME-PKG85 ME-ICP86 ME-XRF12 ME-XRF12p ME-XRF12s ME-ICP82
TiO2, Fe2O3, Al2O3, CaO, Cr2O3, MgO, MnO, Nb2O5, P2O5, Fusion, ICP-AES SiO2, V 2O5, ZrO2, LOI (Other elements available on request) TiO2, Fe2O3, Al2O3, CaO, Cr2O3, MgO, MnO, Nb2O5, P2O5, Fusion, ICP-AES SiO2, V 2O5, ZrO2, LOI (Other elements available on request) TiO2, Fe2O3, Al2O3, CaO, Cr2O3, MgO, MnO, Nb2O5, P2O5, Fusion, ICP-AES SiO2, V 2O5, ZrO2, LOI (Other elements available on request) TiO2, Fe2O3, Al2O3, CaO, Cr2O3, MgO, MnO, Nb2O5, P2O5, Fusion, ICP-AES SiO2, V 2O5, ZrO2, LOI (Other elements available on request)
Zircon Product
ME-ICP83
Ilmenite Product
ME-ICP84
ME-ICP94
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ALS Minerals provides quantitative mineralogical determinations for exploration, mining, metallurgical and environmental industries. Mineralogical analyses are carried out using the MLA (Mineral Liberation Analyser) system which is a scanning-electron microscope system equipped with advanced software and energy dispersive x-ray detectors.
DeTAilS
Batch fee irrespective of number of samples (new ores). Crushing/milling of bore core and uncrushed ore for mineralogical analysis. Price determined by mass of sample. Sizing/cyclosizing into different size fractions. Preparation of 30mm epoxy polished sections for analysis.
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MIN-STD MIN-CRU MIN-SIV MIN-PREP1
DeTAilS
Determination of the mineralogy of Au/Ag/PGM in ore and process samples. Multiple polished sections need to be analysed. Determination of the mineralogy of uranium in ore and process samples. Multiple polished sections need to be analysed. Determination of the mineralogy of Mineral Sands Deposits. Determination of the deportment of Cu-, Ni-, Zn-, Pb-, Mo-, Co-, Ta/Nb-, Sn-, U-, Cr-, Mn- and W-bearing minerals in ore and process samples. Price is determined by grade and multiple polished sections need to be analysed for low grade samples. High Level analysis (textural data included). Low Level analysis (textural data excluded). Determination of the mineralogy of Fe ores and process samples including full quantification of magnetite,hematite and goethite as separate minerals. Determination of the mineralogy of inorganic phases in coal/fly ash. Ore characterisation Mineralogy of coarse particles. Reporting of mineralogical results in basic or interpretive format.
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MIN-PREC MIN-URAN MIN-SAND
* All work subject to formal quotation being issued to Client. ** All prices are indicative only and exclude sizing, polished section preparation and reporting costs.
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GeOCheMiSTry
SPeCiALTy GeOCheMiSTry
COnCenTrATeS MinerALOGy
OTher ServiCeS
DeTAilS
Mineral Abundance (MIN-BMS1) 4-acid Digestion, ICP-MS (ME-MS61) Fire Assay PGM Analysis (PGM-MS23)
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AssyMIN-PKG01
Mineral Abundance (MIN-GEOM) Whole Rock major elements with LOI (ME-XRF06) 30 elements, Lithium Borate Fusion-ICP-MS including rare earth elements (ME-MS81) Volatiles: As-Sb-Hg-Bi-Se-Te by aqua regia-ICP-MS C, S Total Carbon and Sulfur (ME-IR08) Au-Pt-Pd Fire Assay-ICP-MS (PGM-MS23) LithMIN-PKG02 550.00
*Minimum sample weight required is 100g of 75 micron pulp. **A minimum of 20 samples per batch submission is required. ***Mineralogy excludes data on trace minerals.
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In many instances geologists are forced to operate in new geographies with little logistical support and yet are still expected to collect data that is meaningful and insightful. To support such efforts, many ALS facilities now offer a variety of services to help collect and analyse drill samples in a highly-secure and controlled environment. Together these services can provide a streamlined and easy way to collect, store, and retrieve a wealth of information very soon after core is provided to the laboratory.
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ALS Minerals now offers a ground-breaking and unique core photography service. This service allows high quality photographic images of core to be collected on our web-based service for secure sharing and ready pairing with analytical data to aid geological interpretation and communication without return to the core box.
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LOG-COR10 PHO-COR10 PXRF-01 OA-GRA08 SAW-01 STO-COR10
Price ($)
Price on Request
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Truly remote projects require a higher degree of support. Each project has particular demands and no two circumstances are exactly alike. The logistics and expense of sample shipment often drives a need for carefully designed on-site sample preparation. In some situations, on-site analytical capability is required.
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COnCenTrATeS MinerALOGy
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ALS Minerals offers expert construction, supply, management and advice when establishing an on-site laboratory facility at your location. When partnering with ALS Minerals you will have the peace of mind that your design, establishment, commissioning and daily laboratory management will be accomplished to the same high standard that characterises all ALS Minerals facilities.
Once a mineral lab is installed at the mine site, the client will have access to an array of additional services : Consulting Mineralogy Environmental Metallurgical Research and Development Oil Condition Monitoring for the Mining Fleet
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COnCenTrATeS MinerALOGy
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2. ALS will provide the services by exercising the same degree of skill, care and diligence that would be exercised by professional service providers in similar circumstances. 3. The placement of an order for or receipt of samples for analysis based on this Agreement will constitute acceptance of these Terms & Conditions by the client. 4. This Agreement is valid for 30 days from the issue date unless specifically indicated otherwise. 5. ALS reserves the right to review prices at any time if significant changes to our costs are incurred that are beyond our control eg changes in legislative requirements or Client variations to sample numbers, analytes requested, turnaround required, reporting requirements and such. 6. Payment terms are 30 days from invoice date, subject to credit approval, unless otherwise agreed in writing prior to sample submission. To ensure timely release of results, you may wish to contact our credit department prior to submitting samples to check the status of your existing trade account, submit a credit application (available at www.alsglobal.com/MineralDownloads. aspx under Minerals Forms) or arrange for payment prior to our release of results. 7. To the full extent permitted by law ALS excludes all warranties, terms, conditions or undertakings, (terms) whether expressed or implied, in relation to the services, the report, or its contents. Where any legislation implies any terms in this Agreement that cannot be modified or excluded then such terms shall deem to be included. However, to the full extent permitted by law, ALS liability to the Client is limited at ALS option to the reperformance of the service or the refund of the service fee.
8. Without limiting the generality of clause 7, it is agreed that, to the full extent permitted by any applicable laws having jurisdiction, ALS will not be liable to the Client or any other person for any special, indirect or consequential damages arising from the Clients use of ALS services or reports. 9. The Client hereby releases and indemnifies and shall continue to release and indemnify ALS, its officers, employees and agents from and against all actions, claims, proceedings or demands (including any costs and expenses in defending or servicing same) which may be brought against it or them, in respect of any loss, death, injury, illness or damage to persons or property and whether direct or indirect and in respect of any breach of any industrial or intellectual property rights, howsoever arising out of the use of the services or report of ALS.
10. The Client acknowledges that it is the clients sole responsibility to make its own assessment of the suitability for any purpose of the service, report and its contents. 11. The service provided is subject to detection limits and confidence intervals inherent in our current methodology. Because each client is reliant upon assay results for a particular purpose and
Sudbury
1315 Kelly Lake Road Sudbury Ontario P3E 5P5 Tel: 1 705 560 7225 Email: [email protected]
GHANA Kumasi
Cusco
Terrace
2912 Molitor Street, Terrace, BC V8G 3A4 Tel: 1 250 635 3309 Email:[email protected]
Plot 1-4, Block A New Brofoyedu North East Kumasi Tel: 27 11 461 3237 Email:[email protected]
Av. Los Pinos H-1 Distrito de Wanchaq, Cusco Tel: 51 84 23 3406 Email:[email protected]
Lima
IRELAND OMAC
ARGENTINA Mendoza
Thunder Bay
Altos Homos Zapla 1605 Godoy Cruz, Mendoza Tel: 54 261 431 9880 Email:[email protected]
1160 Commerce Street Thunder Bay, Ontario P7E 6E9 Tel:1 807 475 3329 Email:[email protected]
Athenry Road Loughrea, Ireland Tel: 353 91 841 741 Email: [email protected]
Calle 1 LT-1A Mz-D Esq. Calle A Urb. Industrial Bocanegra Callao 1 Tel: 51 1 574 5700 Email:[email protected]
Trujillo
Timmins
LAOS Vientiane
Av. Los Cisnes 109, Urb. Los Pinos Trujillo, La Libertad Tel: 51 44 28 0351 Email:[email protected]
Unit 1, 1 Burma Road, Pooraka Adelaide, South Australia 5095 Tel: 61 8 8359 0890 Email:[email protected]
2090 Riverside Drive, Unit 10 Timmins, Ontario P4R 0A2 Tel: 1 705 360 1987 Email:[email protected]
297 Saphanthong Neua Road PO Box 11289, Vientiane Tel: 856 21 31 3438 Email:[email protected]
Val-dOr
Alice Springs
1324 Rue Turcotte, Val-dOr, Quebec J9P 3X6 Tel: 1 819 825 0178 Email:[email protected]
LIBERIA Monrovia
Loc.Gura Rosiei, Comuna Rosia Montana Jud Alba, 517619 Tel: 40 258 780 395 Email:[email protected]
RUSSIA Chita
Vancouver
Brisbane
32 Shand Street, Stafford Brisbane, Queensland 4053 Tel: 61 7 3243 7222 Email:[email protected]
2103 Dollarton Hwy North Vancouver, BC V7H 0A7 Tel: 1 604 984 0221 Email:[email protected]
MALI Bamako
Whitehorse
Kalgoorlie
78 Mt Sima Road Whitehorse Yukon Y1A 0A8 Tel: 1 867 633 4746 Email:[email protected]
MEXICO
Chihuahua
P.O. Box 54605 Anakheel Area (1), Saleh Atawageri (57) Street Jeddah, 21254 Kingdom of Saudi Arabia Tel: 966 2 251 1911 Email:[email protected]
Karratha
Yellowknife
Sample Delivery: #3 Coronation Drive Mail: PO Box 1919, Yellowknife, NT X1A 2P4 Tel: 1 867 873 5159 Email:[email protected]
Avenida de las Industias No 6500 Col. Zona Industrial Nombre de dios Chihuahua, C.P. 31156 Tel: 52 614 417 9728 Email:[email protected]
[email protected] 61 Brunton Circle Founders View South Modderfontein Johannesburg 1645 Tel: 27 11 608 0555 Email:[email protected]
Mount Isa
Unit 4, 16 Enterprise Road Mt. Isa, Queensland 4825 Tel: 61 7 4740 1700 Email:[email protected]
CHILE Antofagasta
Guadalajara
Orange
Calle Juan Gutemberg 452 Galpon 17 y 18, Antofagasta Tel: 56 2 654 6170 Email:[email protected]
La Serena
FCO. Silva Romero (Antes Jazmn) # 1140 E/R. Michel y Amapola Sector Reforma Colonia San Carlos CP 44460 Guadalajara, Jalisco Mexico Tel: 52 33 3619 7438 Email:[email protected]
SPAIN Seville
Perth
31 Denninup Way, Malaga Perth, Western Australia 6090 Tel: 61 8 9347 3222 Email:[email protected]
Avenida La Fragua 1130 Barrio Industrial Chanar Alto Penuelas, Coquimbo Tel: 56 2 654 6135 Email:[email protected]
Hermosillo
CHINA Guangzhou
Magnolia #16, Esq. Laureles Col. Libertad, Hermosillo Sonora 83130 Tel: 52 662 260 7586 Office: 52 662 218 4403 Email:[email protected]
Poligono Industrial Parque Plata Calle Camino Mozarabe Naves 13 y 15, Camas (Seville) 41900 Tel: 34 955 981 491 Email:[email protected]
SWEDEN Pite
Townsville
14-15 Desma Court, Bohle Townsville, Queensland 4818 Tel: 61 7 4796 0600 Email:[email protected]
Building 12, American Industrial Park 48 Hongmian Avenue, Huadu District Guangzhou, Guangdong,China 510800 Tel: 86 203 687 5966 Email:[email protected]
Zacatecas
BOLIVIA Oruro
Hohhot
Avenida Circunvalacin y Final Campo Jordn s/n. Oruro Tel: 591 2 527 8235 Email:[email protected]
30m West of Hu-Bao Speedway Exit Jinchuang, Hohhot, Inner Mangolia, China Tel: 86 471 360 0886 Email:[email protected]
Transito Pesado S/n Bodega 100, 200, 300 y 400 Frente a Central Camionera Col. Lomas de la Isabelica C.P. 98099, Zacatecas, Zacatecas Tel: 52 492 768 1474 Tel: 52 492 768 1616 Email:[email protected]
TANZANIA Mwanza
Plot No. 28 New Industrial Area Mkuyuni, Mwanza Tel: 255 28 255 0486 Email:[email protected]
MONGOLIA Ulaanbattar
TURKEY Izmir
Hulunbeir
Backside of Mengxi Logistics Park Hailar District, Inner Mongolia, China Tel: 86 470 828 1702 Email:[email protected]
210136 Amono Corporation Building Chingis Avenue, Khan-Uul District Ulaanbaatar Tel: 976 11 343882 Email: info.mongolia@stewartgroupglobal. com
Fatih Mahallesi Ege Caddesi No: 7/B Sarnic Gaziemir Izmir, 35414 Turkey Tel: 90 232 281 7110 Email:[email protected]
Goiania
COLOMBIA Bogota
USA
Avenida Anhanguera Qd 25 Lt 11E, No. 15.060 Setor Santos Dumont Goiania, GO 74.463-350 Tel: 55 62 3088 4800 Email:[email protected]
Parque Agroindustrial Peru, Bodega 4 Funza (Km 2 via Siberia), Bogota - Colombia Tel: 57 1 826 1635 Email:[email protected]
NAMIBIA Swakopmund
Anchorage
Medellin
7011 Old Seward Highway Anchorage, Alaska 99518 Tel: 1 907 349 1789 Email: [email protected]
Porte 629, Blvd Tansoba Tabkom Zone Kossodo, Secteur 25, 11 BP 235 CMS Tel: 226 5035 6077 Email:[email protected]
Bodegas San Bartolome Bodega 3, Carrera 48B No 99 Sur - 59, La Estrella Medellin, Colombia Tel: 57 1 306 9122 Email:[email protected]
Elko
ECUADOR Quito
Ave. Eloy Alfaro N73-93 y Antonio Basantes Tel: 59 32 247 6475 | Fax: 593 2 247 0968
16 Rue Georgette Mourin Parc Deenterprise de la Yahoue Noumea Cedex Normandie BP 30520,988895 New Caledonia Tel: 687 44 1580 Email:[email protected]
2056 Last Chance Road Elko, Nevada 89801 Tel: 1 775 738 2054 Email:[email protected]
Fairbanks
NORWAY Kirkenes
1060 Bush Street Fairbanks, Alaska 99709 Tel: 1 907 452 2188 Email:[email protected]
CANADA
FIJI Suva
[email protected] [email protected]
Reno
4977 Energy Way Reno, Nevada 89502 Tel: 1 775 356 5395 Email:[email protected]
Kamloops
10041 Dallas Drive Kamloops, British Columbia V2C 6T4 Tel: 1 250 573 5700 Email: [email protected]
FINLAND Outokumpu
PERU Arequipa
Winnemucca
Urb. Industrial El Cayro Manzana A, Lote 3, Distrito Paucarpata, Arequipa Tel: 51 54 46 3649 Email:[email protected]
3275 Fountain Way Winnemucca, Nevada 89445 Tel: 1 775 625 4192 Email:[email protected]
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