B1. Bulck S.G PDF
B1. Bulck S.G PDF
B1. Bulck S.G PDF
Bulk SG Permeability
To cite this article: Sudip Bhattacharjee & Rajib B. Mallick (2002) An Alternative Approach for the Determination of Bulk
Specific Gravity and Permeability of Hot Mix Asphalt (HMA), International Journal of Pavement Engineering, 3:3, 143-152, DOI:
10.1080/1029843021000067782
Taylor & Francis makes every effort to ensure the accuracy of all the information (the “Content”) contained in the
publications on our platform. However, Taylor & Francis, our agents, and our licensors make no representations or
warranties whatsoever as to the accuracy, completeness, or suitability for any purpose of the Content. Any opinions
and views expressed in this publication are the opinions and views of the authors, and are not the views of or endorsed
by Taylor & Francis. The accuracy of the Content should not be relied upon and should be independently verified with
primary sources of information. Taylor and Francis shall not be liable for any losses, actions, claims, proceedings,
demands, costs, expenses, damages, and other liabilities whatsoever or howsoever caused arising directly or indirectly
in connection with, in relation to or arising out of the use of the Content.
This article may be used for research, teaching, and private study purposes. Any substantial or systematic reproduction,
redistribution, reselling, loan, sub-licensing, systematic supply, or distribution in any form to anyone is expressly
forbidden. Terms & Conditions of access and use can be found at http://www.tandfonline.com/page/terms-and-
conditions
The International Journal of Pavement Engineering, 2002 Vol. 3 (3), pp. 143–152
Civil and Environmental Engineering Department, Worcester Polytechnic Institute (WPI), Institute Road, Worcester, MA 01609, USA
Downloaded by [University of Waterloo] at 18:56 22 October 2014
The objective of this study was to investigate the use of an alternative method for determination of bulk
specific gravity and estimation of water permeable voids of dense graded HMA mixes. As a part of an
ongoing study on evaluation of permeability of HMA, several dense graded mixes with coarse and fine
gradations from three New England states were compacted to produce mixes at different air voids. The
bulk specific gravities of these mixes were determined using both the saturated surface dry method and
the vacuum seal method. Theoretical maximum densities of these mixes were also determined. Air
voids of the different compacted mixes were estimated from the bulk specific gravity and theoretical
maximum density values. Porosity and permeability tests were also conducted on the mixes. The results
showed that for coarse graded mixes and fine graded mixes with high air voids, the vacuum seal method
provided a better estimation of air voids in a compacted HMA mix. For coarse graded mixes, porosity
can provide a good indication of inter-connectivity of air voids in a compacted HMA mix. Analysis of
the data showed that porosity could provide an excellent indication of permeability of HMA. A porosity
of 7% seemed to be critical—mixes with porosity greater than 7% showed significantly higher
permeability than mixes with porosity lower than 7%. Charts have been provided for selection of proper
gradation and air voids to avoid mixes with excessive permeability.
Keywords: Air voids; Bulk specific gravity; Vacuum seal; Porosity; Permeability
*E-mail: [email protected]
†
Corresponding author. E-mail: [email protected]
ISSN 1029-8436 print/ISSN 1477-268X online q 2002 Taylor & Francis Ltd
DOI: 10.1080/1029843021000067782
144 S. BHATTACHARJEE AND R.B. MALLICK
Bulk Specific Gravity ¼ A={D 2 E 2 ðD 2 AÞ=F} . Step 1: Obtain the bag weight.
. Step 2: Obtain the dry sample weight.
where A ¼ Mass of the dry specimen in air, D ¼ Mass of . Step 3: Place the bag containing the asphalt sample
dry coated specimen, E ¼ Mass of coated specimen under inside the vacuum chamber.
water and F ¼ Specific Gravity of the coating as . Step 4: Close the chamber door. The vacuum pump will
determined at 258C. start automatically and evacuate the chamber to
Unfortunately, the AASHTO T275-89 test method used approximately 117.91 mm Hg.
for sealing of compacted asphalt samples can have poor . Step 5: In approximately two minutes, the chamber
repeatability, high sensitivity to operator involvement and door will open automatically. The sample is completely
training (Buchanan, 2000). Furthermore, there are sealed, ready for water displacement analysis.
currently no specifications for sealing 150 mm diameter . Step 6: Obtain the sealed weight of the sample.
samples. Consequently, few agencies require the use of . Step 7: Water displace the sample using a basket that is
this method. connected to a standard scale.
VOIDS AND PERMEABILITY OF HMA 145
. Step 8: Use the following equation to calculate the bulk TABLE I Mix information
specific gravity of the sample.
State Mix Sieve size (mm) % Passing
A
Bulk Specific Gravity ¼ CT TD 12.5 19 100
B 2 E 2 B2A
FT 12.5 93
9.5 74
4.75 43
where: A ¼ mass of dry specimen in air, g; B ¼ mass of 2.36 30
dry, sealed specimen, g; E ¼ mass of sealed specimen 1.18 22
underwater, g and FT ¼ Apparent specific gravity of 0.6 15
0.3 9
plastic sealing material at 258C (778F), provided by the 0.15 6
manufacturer. 0.075 3.6
TP 12.5 19 100
12.5 96
9.5 83
Downloaded by [University of Waterloo] at 18:56 22 October 2014
TABLE I – continued
4.75 60
2.36 41
1.18 27
0.6 17
0.3 10
0.15 7
0.075 5
VT RT 4 19 100
12.5 99
9.5 82
4.75 57
2.36 37
1.18 24
0.6 16
0.3 10
0.15 6
0.075 3.5
State Mix Target VTM, (%) Sample No. VTM, SSD (%) VTM, vacuum seal (%) Porosity (%) Permeability (cm/s)
CT TD 12.5 5 1 4.47 4.74 7.33 1.83E 2 03
2 5.48 6.26 8.89 2.05E 2 03
3 4.56 5.42 8.14 2.60E 2 03
7 3 6.85 8.10 10.72 6.65E 2 03
12 6.79 8.28 10.73 6.85E 2 03
13 6.53 8.37 10.95 7.47E 2 03
10 1 11.95 11.99 14.01 2.61E 2 02
2 9.06 11.33 14.04 2.54E 2 02
3 8.89 10.98 13.53 2.20E 2 02
TW 9.5 5 1 4.48 4.68 3.48 1.05E 2 04
2 5.30 5.76 3.97 1.73E 2 04
3 4.60 5.05 3.06 1.28E 2 04
7 2 6.66 7.10 5.18 3.04E 2 04
Downloaded by [University of Waterloo] at 18:56 22 October 2014
TABLE II – continued
State Mix Target VTM, (%) Sample No. VTM, SSD (%) VTM, vacuum seal (%) Porosity (%) Permeability (cm/s)
method, particularly with compacted mixes at relatively percent of water accessible air voids in HMA, especially
high air voids (such as 10%). for coarse graded mixes.
Figure 3a – c, shows the difference between vacuum seal
method VTM and porosity data for 9.5,12.5, 19 mm
Analysis of Laboratory Permeability Testing
NMAS mixes, respectively. The plots show that the
(on Laboratory Compacted Samples) Data
difference is positive and very low at lower air voids. At
high air voids (10% VTM), for the fine mixes, the Water flows through accessible voids or pore spaces in a
difference is positive, indicating the presence of pavement. Hence, the rate of flow must be related to the
inaccessible air voids. For the coarse mixes, at high air amount of water accessible voids, or effective porosity, in
voids, the difference is either very small or negative, some way. Therefore, the coefficient of permeability must
indicating the presence of highly inter-connected air be a function of porosity. Table II shows the effective
voids, which are accessible to water. Negative differences porosity versus permeability data, as obtained from
can also indicate a less than optimum asphalt coating that laboratory testing. The best model for defining the
would ultimately allow water to penetrate into the relationship between effective porosity and permeability
aggregate grain. Therefore, the vacuum seal method seems to be one of exponential in nature, as shown in Fig. 4
seems to be a good method for getting an indication of (considering data from 9.5 to 12.5 mm NMAS mixes
only). Figure 4 shows two relationships: VTM versus
permeability ðR 2 ¼ 0:55Þ and effective porosity
versus permeability ðR 2 ¼ 0:80Þ: The effective porosity
versus permeability model is significantly better than the
VTM versus permeability model. If one considers
the effective porosity versus permeability model, then the
critical porosity corresponding to a critical permeability
can be determined. Since, in general, permeability data for
HMA is highly variable, and the nature of the
permeability –porosity plot is exponential, it is logical to
consider the value of permeability in terms of 10X, rather
than in terms of exact value. As recommended by Florida
Department of Transportation (DOT) researchers (Chou-
bane et al., 1998), considering a critical permeability of
1023 cm/s, a critical porosity of 7% is determined (from
Fig. 4). Therefore, mix design samples can be checked for
permeability potential by conducting porosity tests on
samples compacted to construction voids (as determined
FIGURE 2 Plot of VTM versus difference of vacuum seal method VTM by SSD method), and a maximum porosity value of 7%
and SSD VTM. can be recommended.
VOIDS AND PERMEABILITY OF HMA 149
Downloaded by [University of Waterloo] at 18:56 22 October 2014
FIGURE 3 (a) Plot of vacuum seal VTM versus difference between vacuum seal VTM and porosity for 9.5 mm mixes; (b) Plot of vacuum seal VTM
versus difference between vacuum seal VTM and porosity for 12.5 mm mixes; (c) Plot of vacuum seal VTM versus difference between vacuum seal
VTM and porosity for 19 mm mixes.
TABLE III Results of multiple regression analysis with mix gradation, air voids and porosity
Regression summary
Porosity vs. 2 independents
Row exclusion: perm #1_12.5_9.5.svd
Count 68
Num. Missing 3
jRj 0.897
R squared 0.804
Adjusted R squared 0.798
RMS residual 1.406
ANOVA table
Porosity vs. 2 independents
Row exclusion: perm #1_12.5_9.5.s.vd
DF Sum of squares Mean square F-value P-value
Regression 2 526.694 263.347 133.281 ,0.0001
Downloaded by [University of Waterloo] at 18:56 22 October 2014
theoretical maximum density) can be determined. A list of of 7 per percent corresponds to VTM of 7%. Most
critical air voids, for mixes with different percent passing experiences from the past (in the pre-Superpave era) has
the 2.36 mm sieve, is shown in Table IV. The critical air been with mixes with 40 –45% passing the 2.36 mm sieve,
voids range from 5 to 7.5 corresponding to PP2.36 of and a VTM of 7% has often been recommended and used,
25 to 45. One can use this table to specify maximum without any significant permeability or durability (related
construction air voids for a specific mix. to excessive aging) problem. Therefore, the selection of
From Fig. 5 it can be noted that for a mix with 7% porosity as a critical porosity seems to be well
approximately 45% passing the 2.36 mm sieve, a porosity justified.
From Fig. 6 one can determine the critical PP2.36 value
for any specific air voids. Table V shows a list of critical
PP2.36 for a range of air voids. One can use the values
from this table to select suitable gradation(s) during mix
design for a specific construction air voids. For example, if
it is known that realistically air voids below 6% cannot be
achieved, and then one can select a specific PP2.36
FIGURE 5 Plot of air voids versus porosity for different percent passing
the 2.36 mm sieve.
TABLE V List of critical percent passing the 2.36 mm sieve for specific relationship with permeability, perhaps porosity is a good
air voids mix design parameter candidate also. This argument
becomes stronger when one considers the coefficient of
Air Voids Allowable percent passing the 2.36 mm sieve
variation of the permeability and the porosity tests.
5 .25 Table VI shows the coefficient of variation (CV) for each
6 .31
7 .41 set of samples as well as average CV for porosity and
8 .45 permeability data. The average CV for permeability
testing is about three times the average CV of porosity.
Hence, as a regular test procedure, because of better
(greater than 31%) such that the porosity of the resulting repeatability, porosity seems to be more appropriate than
mix is below 7% air voids. permeability. Also, determination of porosity is simple
A question that arises from the analysis of the data is and rapid as compared to laboratory permeability test.
that which parameter should be used during mix design to Since asphalt laboratories can use the vacuum sealing
Downloaded by [University of Waterloo] at 18:56 22 October 2014
prevent mixes from being excessively permeable—is it device to determine the bulk specific gravity of
the permeability value or is it the porosity value? compacted HMA, the determination of porosity will be
Obviously, measuring permeability is a more direct just an additional step when testing for bulk specific
approach. However, since porosity shows a very good gravity.
Target VTM Porosity Coefficient of variation, porosity Coefficient of permeability Coefficient of variation, coefficient of permeability
(%) (%) (%) (cm/s) (%)
5 7.3 9.59 0.001826 18.52
8.8 0.002047
8.13 0.002602
7 10.7 1.21 0.006647 6.14
10.7 0.006849
10.9 0.007471
10 14.0 2.09 0.026135 9.05
14.0 0.025357
13.5 0.021963
5 3.8 20.38 0.000294 31.96
3.1 0.000307
4.7 0.000505
7 6.6 5.89 0.000118 70.49
6.4 0.00087
5.9 0.000908
10 8.3 15.02 0.00318 39.63
8.0 0.00183
10.5 0.00156
5 3.4 12.97 0.000104 25.61
3.9 0.000172
3.0 0.000128
7 5.1 23.20 0.000304 18.02
5.0 0.000371
7.5 0.000438
10 9.2 5.13 0.001808 11.43
8.9 0.002024
9.8 0.002273
5 4.0 6.60 0.000366 15.46
4.2 0.000475
3.7 0.000368
7 6.4 4.29 0.000904 18.99
6.8 0.000748
6.4 0.000617
10 11.9 1.03 0.00477 23.71
12.0 0.00776
11.8 0.00683
5 5.3 21.15 0.000399 24.70
3.4 0.000643
4.3 0.000632
7 8.3 3.46 0.002037 46.95
8.8 0.004096
8.3 0.001842
10 12.7 8.26 0.013027 41.15
14.0 0.025045
11.90 0.012860
Average 9.35 26.79
152 S. BHATTACHARJEE AND R.B. MALLICK
4. Porosity is significantly affected by percent of material and Methods of Sampling and Testing, Part II Tests, 15th Ed.,
Adopted by the American Association of State Highway and
passing 2.36 mm sieve. Transportation Officials.
AASHTO T275-89 (1990). Standard Method of Test for Bulk Specific
Based on the above conclusions the following Gravity of Compacted Bituminous Mixes. Using Paraffin Coated
Specimens, Standard Specifications for Transportation Materials and
recommendations are made: Methods of Sampling and Testing, Part II Tests. 15th Ed., Adopted by
the American Association of State Highway and Transportation
1. Use of the vacuum seal method should be further Officials.
AASHTO T209-99. Theoretical maximum specific gravity and density of
explored for routine bulk specific gravity testing of bituminous paving mixtures. Standard Specifications for Transpor-
HMA mixes. tation Materials and Methods of Sampling and Testing, Part II Tests,
2. Since the vacuum seal method leaves the samples 15th Ed., Adopted by the American Association of State Highway
and Transportation Officials.
intact after testing, this method should be used for bulk AASHTO TP4-97. Standard method for preparing and determining the
specific gravity testing of cold recycled mixes. density of Hot Mix Asphalt specimens by means of SHRP Gyratory
3. Use porosity as an indicator of mix permeability. Compactor. AASHTO provisional standards. Approved for publi-
cation by the AASHTO sub committee on materials.
4. Estimate porosity from mix gradation at specific air ASTM D130-01. Standard Test Method for Bulk Specific Gravity and
voids and use the estimated porosity to select Density of Compacted Bituminous Mixes Using Automatic Vacuum
gradation or desirable construction air voids. Sealing Method. American Society for Testing and Materials.
Bear, J. (1972) Dynamics of Fluid in Porous Media (Dover Publication,
5. Conduct porosity test on mix design samples at Inc., New York).
construction air voids and make sure that the critical Brown, R.E., Decker, D., Mallick, R.B. and Bukowski, J. (1999)
porosity is not exceeded. Superpave Construction Issues and Early Performance Evaluations.
Journal of Asphalt Paving Technologists 68, 613 –660.
Buchanan, M. Shane (2000) An evaluation of selected methods for
measuring the bulk specific gravity of compacted hot mix asphalt
(HMA) mixes. Journal of Association of Asphalt Paving Technol-
ogists 69, 2000.
DISCLAIMER Choubane, B., Page, G.C. and Musselman, J.A. (1998) Investigation of
water permeability of coarse graded superpave pavements. Journal of
the Asphalt Paving Technologists 67, 254 –276.
This paper, prepared in cooperation with the New England Florida DOT Specification (FM 5-565).
Transportation Consortium, does not constitute a standard, Mallick, R.B., Cooley, L.A., Teto, M. and Bradbury, R. (2001)
specification or regulation. The contents of this paper Development of a simple test for evaluation of in-place permeability
of asphalt mixes. International Journal of Pavement Engineering.
reflect the views of the authors who are responsible for the 2(2), 67– 83.
facts and the accuracy of the data presented herein. The Operator’s guide, Copyright December 2000, version 8, CoreLoke,
contents do not necessarily reflect the views of the New Instrotek, Incorporated.
Roberts, F.L., Kandhal, P.S., Brown, E.R., Lee, D. and Kennedy, T.
England Transportation Consortium or the Federal High- (1996) Hot Mix Asphalt Materials, Mixture Design and Construction
way Administration. (NAPA Education Foundation, Lanham, MA).