International University, Vietnam National University - HCMC 1
GENERAL CHEMISTRY LABORATORY
DATA SHEET
EXPERIMENT 1: CHEMICAL REACTIONS
Group: ______________ Section: _____1________Date: ______________
Group members: _______________________________
_______________________________
_______________________________
_______________________________
Instructor’s/TA’s signature and comments:
Expt. 1 Expt. 6
Expt. 2 Expt. 7
Expt. 3 Expt. 8
Expt. 4 Expt. 9
Expt. 5 Approval
International University, Vietnam National University - HCMC 2
GENERAL CHEMISTRY LABORATORY
1. Reactions of Cu2+
Reaction Observation
0.5M CuSO4
+ 2M NaOH
0.5M CuSO4
+ 2M NH4OH
0.5M CuSO4
0.5M K4[Fe(CN)6]
2. Reactions of silver halides
Reaction Observation
0.5M KCl
+ 0.1M AgNO3
0.5M KCl
+ 0.1M AgNO3
+ 2M NH4OH
0.5M KBr
+ 0.1M AgNO3
0.5M KBr
+ 0.1M AgNO3
+ 2M NH4OH
0.5M KI
+ 0.1M AgNO3
0.5M KI
+ 0.1M AgNO3
+ 2M NH4OH
3. Reactions of H2O2
Reaction Observation
0.1M KMnO4
+ 2M H2SO4
+ H2O2
0.1M KI
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GENERAL CHEMISTRY LABORATORY
+ 2M H2SO4
+ H2O2
H2O2
+ MnO2
4. Reactions of Nitrate
Reaction Observation
1M NaNO3
+ FeSO4
+ concentrated
H2SO4
1M NaNO2
+ FeSO4
+ concentrated
H2SO4
1M NaNO3
+ FeSO4
+ concentrated
CH3COOH
5. Reactions of KMnO4
Reaction Observation
0.5M Na2SO3
+ 2M H2SO4
+ 0.1M KMnO4
0.5M Na2SO3
+ 6N NaOH
+ 0.1M KMnO4
0.5M Na2SO3
+ H2O
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GENERAL CHEMISTRY LABORATORY
+ 0.1M KMnO4
6. Reaction of Potassium Dichromate (K2Cr2O7)
Reaction Observation
2M K2Cr2O7
+ 6M H2SO4
+ C2H5OH
7. A. Reactions of Fe3+
Reaction Observation
0.5M FeCl3
+ 0.5M KCN
0.5M FeCl3
+ 0.1M KSCN
0.5M FeCl3
+ 2M KOH
0.5M FeCl3
+ 0.5M K4[Fe(CN)6]
0.5M FeCl3
+ 2M NH4OH
7. B. Reactions of Fe2+
Reaction Observation
0.5M FeSO4
+ 0.1M KSCN
0.5M FeSO4
+ 2M KOH
0.5M FeSO4
+ 0.5M K4[Fe(CN)6]
0.5M FeSO4
+ 2M NH4OH
8. Reactions of Al3+
Reaction Observation
0.5M Al2(SO4)3
+ 2M NaOH
0.5M Al2(SO4)3
+ 2N NaOH
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GENERAL CHEMISTRY LABORATORY
+ 2M HCl
0.5M Al2(SO4)3
+ 2M NaOH
+ 2M NaOH
9. Flame test
Solution Dominant flame color
LiCl
NaCl
KCl
CaCl2
BaCl2
DATA SHEET
EXPERIMENT 2: pH AND BUFFERS
Group: ______________ Section: _____2________Date: ______________
Group members: _______________________________
_______________________________
_______________________________
_______________________________
Instructor’s/TA’s signature and comments:
Expt. 1 Expt. 4
International University, Vietnam National University - HCMC 6
GENERAL CHEMISTRY LABORATORY
Expt. 2 Expt. 5
Expt. 3 Approval
International University, Vietnam National University - HCMC 7
GENERAL CHEMISTRY LABORATORY
1. pH OF DEIONIZED WATER
Observed pH
Time
(second) 1st 2nd
(Group___) (Group___)
0
20
40
60
80
100
120
140
160
2. pH OF STRONG ACID
Measured pH
Solution Theoretical pH
1st 2nd
(Group___) (Group____)
10 mL of 0.1M HCl
Add 90 mL of distilled
water
Add 10 mL of
0.1M NaOH
Add 90 mL of
0.01M NaOH
3. pH OF WEAK ACID
Measured pH
Solution st
1 2nd Averaged Ka
(Group___) (Group____)
0.1M acetic acid
0.01M acetic acid
0.001M acetic acid
4. pH OF SALTS
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GENERAL CHEMISTRY LABORATORY
Measured pH
Solution Predicted pH 1 st
2nd
(Group____) (Group____)
0.1M NaCl
0.1M CH3COONa
0.1M NH4Cl
5. pH OF BUFFERS
Volume (mL) Volume (mL) Measured pH
Calculated
Buffer 0.1M 0.1M Acid Base
pH 1st 2nd
CH3COOH CH3COONa
(Group__) (Group__)
A 10.0 40.0
B 40.0 10.0
C 25.0 25.0
Part I: Addition of 10 drops 0.1 M HCl
pH after adding 10 Total volume HCl (drops) to change
Buffer pH from the start, pHo
drops HCl pH by one unit (pHo-1)
Part II: Addition of 10 drops 0.1 M NaOH
pH after adding 10 Total volume NaOH (drops) to change
Buffer pH from the start, pHo
drops NaOH pH by one unit (pHo+1)
C
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GENERAL CHEMISTRY LABORATORY
DATA SHEET
EXPERIMENT 3: REDOX TITRATION
Group: _____________ Section: _____3_________ Date: ____________
Group members: _______________________________
_______________________________
_______________________________
_______________________________
Instructor’s/TA’s signature and comments:
Expt. 1 Expt. 3
Expt. 2 Expt. 4
Approval
International University, Vietnam National University - HCMC 10
GENERAL CHEMISTRY LABORATORY
1. TITRATION OF KMnO4 SOLUTION WITH STANDARD H2C2O4 SOLUTION
Trial # Burette reading (mL) Volume of KMnO4 (mL) Normality of KMnO4 (N)
1 -
2 -
Average Normality of KMnO4 = ____________ (N)
2. TITRATION OF UNKNOWN CONCENTRATION H2C2O4 SOLUTION WITH STANDARD
KMnO4 SOLUTION
Trial # Burette reading (mL) Volume of KMnO4 (mL) Normality of H2C2O4 (N)
1 -
2 -
Average Normality of H2C2O4 =_______ (N)
3. TITRATION OF UNKNOWN CONCENTRATION FeSO4 SOLUTION WITH STANDARD
KMnO4 SOLUTION
Trial # Burette reading(mL) Volume of KMnO4 (mL) Normality of FeSO4(N)
1 -
2 -
Average Normality of FeSO4 =_______ (N)
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GENERAL CHEMISTRY LABORATORY
DATA SHEET
EXPERIMENT 4: CHEMICAL EQUILIBRIUM
Group: _____________ Section: ______4________ Date: ____________
Group members: _______________________________
_______________________________
_______________________________
_______________________________
Instructor’s/TA’s signature and comments:
Expt. 1 Expt. 4
Expt. 2 Expt. 5
Expt. 3 Approval
International University, Vietnam National University - HCMC 12
GENERAL CHEMISTRY LABORATORY
1. ACID/BASE EQUILIBRIA
Equilibrium System: 2CrO42 + 2H+(aq) ⇌ Cr2O72 + H2O(l)
Description of Predicted outcome Observation
conditions
Initial solution
+ Conc. HCl
+ 6 N NaOH
2. EQUILIBRIA OF ACID/BASE INDICATORS
Equilibrium System: H(MV)(aq) + H2O(l) ⇌ H3O+(aq) + MV(aq)
Addition Predicted outcome Observation
None (control)
6 M HCl
6 M NaOH
6 M HCl
3. COMPLEX ION FORMATION
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GENERAL CHEMISTRY LABORATORY
Equilibrium System: Fe3+ + SCN ⇌ [Fe(SCN)]2+
Addition Predicted outcome Observation
None
(control)
0.01M FeCl3
0.01 M KSCN
6M NaOH
Cold
Hot
0.1M AgNO3
4. EQUILIBRIA OF PRECIPITATION REACTIONS
Equilibrium System: Ca2+(aq) + C2O42(aq) ⇌ CaC2O4(s)
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GENERAL CHEMISTRY LABORATORY
Addition Predicted outcome Observation
Test tube 1:
0.1 M Na2C2O4
Test tube 2:
+ 0.1 M H2C2O4
Test tube 2:
+ 6 M HCl
Test tube 2:
+ 6 M NH4OH
5. TEMPERATURE EFFECTS ON EQUILIBRIA
Equilibrium System: Co(H2O)6 2+(aq) + 4Cl(aq) ⇌ CoCl4 2(aq) + 6H2O(l)
Description of
Predicted outcome Observation
conditions
Nothing
changed
(control)
Hot water bath
Ice-water bath
International University, Vietnam National University - HCMC 15
GENERAL CHEMISTRY LABORATORY
DATA SHEET
EXPERIMENT 5: FACTORS AFFECTING
REACTION RATE
Group: _____________ Section: _____5_________ Date: _____________
Group members: _______________________________
_______________________________
_______________________________
_______________________________
Instructor’s/TA’s signature and comments:
Expt. 1 Expt. 3
Expt. 2 Approval
International University, Vietnam National University - HCMC 16
GENERAL CHEMISTRY LABORATORY
1. EFFECT OF CONCENTRATION ON REACTION TIME
Reaction 1:
__________________________________________________
Reaction 2:
__________________________________________________
Calculate the initial concentrations of I- and S2O82- ions:
Mixture # 5:
[I-] =
[S2O82-] =
Mixture Iodide ion Peroxydisulfate Time in seconds
Mixture Iodide ion Peroxydisulfate Time in seconds
10
11
2. EFFECT OF TEMPERATURE ON THE REACTION RATE
Reaction System:
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GENERAL CHEMISTRY LABORATORY
Description of Predicted outcome Observation Reaction time
conditions
Room
temperature
500C
900C
3. EFFECT OF A CATALYST ON THE REACTION RATE (30 pts)
Reaction System:
Trial Description of Predicted outcome Observation (Reaction rate)
conditions
1 + MnCl2
2 + MnO2
3 + NaCl
4 + CaCl2
5 + Zn
6 + KNO3
7 + Fe(NO3)3
