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    Astm D2163-91

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    Johapi Joha Sana
    This document summarizes ASTM Method D2163-91 for analyzing the composition of liquefied petroleum gases and propene concentrates. The method analyzes propane, propene, butane and other components at levels above 0.1% by volume. It uses a single channel micro GC with a short methyl silicone column for fast analysis at 48°C to identify 11 different hydrocarbon components, including various butane isomers and low levels of butadiene.

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    Astm D2163-91

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    Johapi Joha Sana
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    This document summarizes ASTM Method D2163-91 for analyzing the composition of liquefied petroleum gases and propene concentrates. The method analyzes propane, propene, butane and other components at levels above 0.1% by volume. It uses a single channel micro GC with a short methyl silicone column for fast analysis at 48°C to identify 11 different hydrocarbon components, including various butane isomers and low levels of butadiene.

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    ASTM D2163-91

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    This document summarizes ASTM Method D2163-91 for analyzing the composition of liquefied petroleum gases and propene concentrates. The method analyzes propane, propene, butane and other components at levels above 0.1% by volume. It uses a single channel micro GC with a short methyl silicone column for fast analysis at 48°C to identify 11 different hydrocarbon components, including various butane isomers and low levels of butadiene.

    Copyright:

    Attribution Non-Commercial (BY-NC)
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
    1K views1 page

    Astm D2163-91

    Uploaded by

    Johapi Joha Sana
    This document summarizes ASTM Method D2163-91 for analyzing the composition of liquefied petroleum gases and propene concentrates. The method analyzes propane, propene, butane and other components at levels above 0.1% by volume. It uses a single channel micro GC with a short methyl silicone column for fast analysis at 48°C to identify 11 different hydrocarbon components, including various butane isomers and low levels of butadiene.

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    Attribution Non-Commercial (BY-NC)
    Download as PDF, TXT or read online from Scribd
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    ASTM Method D2163-91

    Liquefied Petroleum (LP) Gases and Propene Concentrates


    Ethane, propene, propane, butanes and butenes.

    ASTM Method D2163-91: Analysis of Liquefied Petroleum (LP) Gases and Propene Concentrates
    Method Overview: This method analyzes the composition of LP gases. Analysis of propane, propene and butane at 0.1 volume % and above are required.

    Single channel analysis of LPG, 14 m x 0.15, 2.0 mm methyl silicone, 48_C isothermal.
    Analysis done by Agilent G2890A micro GC and short column for fast analysis. 1. Nitrogen 2. Ethane 3. Propylene 4. Propane 5. Isobutane 6. 1-butene/isobutylene 7. Butane 8. trans-2-butene 9. cis-2-butene 10. isopentane 11. 1-pentene 12. Pentane 30 40 50 60 2 5 6 3 1 30 10 11 12 7 8 9 70 80 90 90 100 10 100 110 11 110 seconds 120 35 40 2

    C4 isomers including butadiene at low levels.


    1. i-Butane 2. Butane 3. Butenes 4. 1,3-Butadiene 5. Ethylacetylene 1 2 3 Column: Oven: Carrier: Inlet: 4 Detector: Sample: HP-PLOT Al2O3 KCl," 50 m x 0.53 mm x 15 m (Agilent part No. 19095P-K25) 120_C (3 min), 10_C/min to 180_C Hydrogen, 33 cm/sec, constant flow 250_C, split flow 200 ml/min FID, 250_C 0.25 cc sampling valve 5

    NOTE: This chromatogram illustrates that, even with very long columns, butadiene reactions are eliminated using the HP-PLOT Al2O3 KCl column.

    7 min

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